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Alpha Analytical, Inc.* <br /> C 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044• (775) 355-0406 FAX • 1-800-283-1183 <br /> Date: OC Summary Report Work Order: <br /> 10-Nov-03 03110343 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: D:\HPCHEM\MS10\DATA\031104\03110439.D Batch ID:MS10W1104C Analysis Date: 11104/2003 20:55 <br /> Sample ID: MBLK MS10WI104C Units: pg/L Run 10:GCIMSD_10_031104B Prep Dale: 11/04/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %aREC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> b Chloromethane NO 2 <br /> Vinyl chloride NO 1 <br /> Chloroethane NO 1 <br /> Bromomelhane NO 1 <br /> j Trichlorofluoromethane NO 1 <br /> 1,1-Dichloroethene NO 1 <br /> Tertiary Butyl Alcohol (TBA) NO 5 <br /> Dichloromethane NO 2 <br /> trans-1,2-Dichloroethene NO 1 <br /> ' Methyl tart-butyl ether(MTBE) ND 0.5 <br /> 1,1-Dichloroethane NO 1 <br /> Di-isopropyl Ether(DIPE) NO 1 <br /> cis-1,2-Dichloroethene NO 1 <br /> Chloroform NO 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) NO 1 <br /> N 1,2-Dichloroethane ND 1 <br /> t 1,1,1-Trichloroethane NO 1 <br /> Carbon tetrachloride NO 1 <br /> Benzene NO 0.5 <br /> 6 Tertiary Amyl Methyl Ether(TAME) NO 1 <br /> 1,2-Dichloropropane NO 1 <br /> Trichloroethene NO 1 <br /> Bromodichloromethane NO 1 <br /> cis-1,3-Dichloropropene ND 1 <br /> ! Vans-1,3-Dichloropropene NO 1 <br /> E 1,1,2-Trichloroethane NO 1 <br /> f Toluene NO 0.5 <br /> Dibromochloromethane NO 1 <br /> ( Tetrachloroethene NO 1 <br /> 1 Chlorobenzene ND 1 <br /> ] Ethylbenzene NO 0.5 <br /> m,p-Xylene NO 0.5 <br /> ( Bromoform NO 1 <br /> E o-Xylene NO 0.5 <br /> E 1,1,2,2-Tetrachloroethane ND 1 <br /> 1,3-Dichlorobenzene ND 1 <br /> 1,4-Dichlorobenzene ND 1 <br /> 1,2-Dichlorobenzene NO 1 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW0260B <br /> File ID: D:\HPCHEM\MS10\DATA\031104\03110437.D Batch ID:MSlOW1104C Analysis Date: 11/04/2003 20:13 <br /> Sample ID: LCS MSlOW1104C Units:pg/L Run ID:GC/MSD_10 0311048 Prep Date: 11/0412003 <br /> Analyte Result PQL SpkVal SpkReNal %,REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> 1,1-Dichloroethene 10.1 1 10 101 80 120 <br /> Benzene 9.62 0.5 10 96 83 119 <br /> Trichloroethene 10.1 1 10 101 76 127 <br /> Toluene 9.37 0.5 10 94 80 120 <br /> Chlorobenzene 9.76 1 10 98 76 124 <br /> Ethylbenzene 9.78 0.5 10 98 80 120 <br /> m,p-Xylene 19.7 0.5 20 99 77 125 <br /> o-Xylene 9.71 0.5 10 97 77 124 <br /> I <br />