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CALIFORNIA LABORATORY SERVICES <br /> Page 6 of 8 06/03/13 15:00 <br /> Alpha Analytical,Inc.-Sparks Project: SGE13051542 <br /> 255 Glendale Ave.;Suite 21 Project Number: SGE13051542 CLS Work Order#:CWE0556 <br /> Sparks,NV 89431 Project Manager: Reyna Vallejo COC#: <br /> Organochlorine Pesticides by EPA Method 8081A - Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch CW03416-LUFT-DHS GCW <br /> Blank(CW03416-BLKI) Prepared:05/28/13 Analyzed:05/29/13 <br /> Aldrin ND 1.0 µg/kg <br /> alpha-BHC ND 2.0 " <br /> beta-BHC ND 10 " <br /> delta-BHC ND 10 " <br /> gamma-BHC(Lindane) ND 10 " <br /> Chlordane-technical ND 20 " <br /> 4,4'-DDD ND 15 " <br /> 4,4'-DDE ND 15 " <br /> 4,4'-DDT ND 15 " <br /> Dieldrin ND 1.0 " <br /> Endosulfan I ND 15 " <br /> Endosulfan II ND 15 " <br /> Endosulfan sulfate ND 15 " <br /> Endrin ND 15 " <br /> Endrin aldehyde ND 15 " <br /> Heptachlor ND 5.0 " <br /> Heptachlor epoxide ND 2.0 " <br /> Methoxychlor ND 15 " <br /> Mirex ND 10 " <br /> Toxaphene ND 20 <br /> Surrogate:Tetrachloro-meta-xylene 5.46 8.33 65 46-139 <br /> Surrogate:Decachlorobiphenyl 7.43 8.33 89 52-141 <br /> LCS(CW03416-BS1) Prepared:05/28/13 Analyzed:05/29/13 <br /> Aldrin 13.1 1.0 µg/kg 16.7 78 47-132 <br /> gamma-BHC(Lindane) 12.2 10 16.7 73 56-133 <br /> 4,4'-DDT 15.5 15 16.7 93 46-137 <br /> Dieldrin 15.1 1.0 16.7 90 44-143 <br /> Endrin 13.1 15 16.7 79 30-147 <br /> Heptachlor 11.9 5.0 16.7 71 33-148 <br /> Surrogate:Tetrachloro-meta-.xylene 6.14 8.33 74 46-139 <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www.californialab.com 916-638-7301 Fax: 916-638-4510 <br />