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r-_ <br /> I� <br /> GeoAnal ficai Laboratories' Inc. <br /> Y <br /> f <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 ,Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# $135-20 Oxygenates ip <br /> Date.- 5/16/03 <br /> i <br /> Thorpe Oil Project: Thorpe's Yard- Resarnple 0 Date Aec'd: 5/15/03 <br /> PO Box 357 Date Started: 5/16/03 <br /> Lodi CA 95241 PO# <br /> Ddte Completed:5/16/03 <br /> ! Date Sampled: 3/15/03 <br /> k <br /> Sampler: R_Azevedo(Geo) , <br /> Sample Iii] Lala ID RL Method Analyte Ik :I Results Units <br /> r <br /> Dispenser#6®9' P200723 10 82600 Meth <br /> y] Cert-butyl ether(NYSE) (VD ug/Kfi <br /> i 400 Ethanol ND <br /> 200 Cert-Butanol ND <br /> 10 di-lsopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether`(ETBE) ND <br /> 10 tent-Amyl methyl ether(TAME) ND <br /> E i <br /> Siuroga5e Aunt Spiked Amnt Ree. %Reoovery QC Limit% <br /> 1,2-Did-daroethane-d„ 10 20.3 101.5 66-133 <br /> 2-Bronw-i-chloropropane 20 23.1 115.5 63-139 <br /> 4-Bromofluorobenzene 20 20.5 102.5 64-136 <br /> Dispenser#109' P200724 10 8260B Methyl terk-bwyl ether(MTBE) ND AR/l� <br /> 400 Ethanol 1' ND <br /> 200 tert Butanol 11 ND <br /> 10 di-isopropyl ether(Dn;,E) ND <br /> 10 Ethyl Cert-butyl ethei.(ETRE) ND <br /> 10 tent-Arnyl methyl ether(TAME) NO <br /> if I <br /> Surrogate Aunt Spiked A uit Rec. %Recovery QC Limit% <br /> 1r2-Oichloroeth=e-d4 20 20.1 100.5 66-133 <br /> 2-$Tomo-l-chforoprapartie 20 23.0 115.0 63-139 <br /> 4-Bromolluorobenzene 20 19-0 95.0 64-136 i 1 <br /> ?l <br /> If <br /> I <br /> j <br /> i <br /> II � <br /> f <br /> ano D'Onaf <br /> Donna Keller <br /> Chemist Certification#1157 Laboratory Director a <br /> S0/Z0 30Vd 039 9T60ZL560Z Lb :9T b00Z/0x/£0 <br />