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110 2nd Avenue S 1h,#D7,Pacheco,CA 94553-5560 <br /> i McCampbell Anailcal, Inc.-T TelepMne: 8-1620 F.:925-798-1622Website:www.mcca com E mmec <br /> -mail: ain® ampbell.com <br /> ' Clayton Group Services Client Project ID: #70-05628.00 Date Sampled: 04/14/05 <br /> Date Received: 04/15/05 <br /> 6920 Koll Center Pkwy, Ste.216 <br /> Client Contact: Craig Pelletier Date Extracted: 04/15/05 <br /> ' Pleasanton, CA 94566 Client P.O.: Date Analyzed: 04/19/05 <br /> Volatile Organics by P&T and GUMS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0504252 <br /> ' Lab ID 0504252-018A <br /> Client ID SB-5 2-2.5' <br /> Matrix Soil <br /> gmg Compound Concentration" DF R`'L,n' Compound ConcentrationDF <br /> Acetone ND 1.0 0.05 Acrolein(Propenal) ND 1.0 0.05 <br /> Acxylonitrile ND 1.0 0.02 tert-Am I methyl ether TAME ND 1.0 0.005 <br /> Benzene ND 1.0 0.005 Bromobenzene ND 1.0 0.005 <br /> Bromochlommethane ND 1.0 0.005 Bromodichlommethane ND 1.0 0.005 <br /> Bromoform ND 1.0 0.005 Bromomethane ND 1.0 0.005 <br /> 2-Butanone EK ND 1.0 0.02 t-Butyl alcohol A ND 1.0 0.025 <br /> ' <br /> n-Butyl benzene ND 1.0 0.005 sec-Butyl benzene ND 1.0 0.005 <br /> tert-Butyl benzene ND 1.0 0.005 Carbon Disulfide ND 1.0 0.005 <br /> Carbon Tetrachloride ND 1.0 0.005 Chlombenzene ND 1.0 0.005 <br /> Chloroethane ND 1.0 0.005 1 2-Chloroeth 1 Vinyl Ether ND 1.0 0.01 <br /> Chloroform ND 1.0 0.005 Chloromethane ND 1.0 0.005 <br /> 2-Chlorotoluene ND 1.0 0.005 4-Chlorotoluene ND 1.0 0.005 <br /> Dibromochloromethane ND 1.0 0.005 1,2-Dibromo-3chloro ro ane ND 1.0 0.005 <br /> 1,2-Dibromoethme DB ND 1.0 0.005 Dibromomethane ND 1.0 0.005 <br /> 1,2-Dichlorobenzene ND 1.0 0.005 1,3-Dichlorobenzene ND 1.0 0.005 <br /> 1,4-Dichlorobenzene ND 1.0 0.005 Dichlorodifluoromethane ND 1.0 0.005 <br /> 1,1-Dichlomethane ND LO 0.005 1,2-Dichlomethme 1,2-DCA ND 1.0 0.005 <br /> IJ-Diehloroethene ND LO 0.005 cis-1,2-Diehloroethme ND 1,0 0.005 <br /> [tans-1,2-Dichloroethene ND 1 1.0 0.005 1 1,2-Dichloro ro ane ND LO 1 0.005 <br /> 1,3-Dichloro ro ane ND 1.0 0.005 1 2,2-Dichloro ro ane ND 1.0 0.005 <br /> 1,1-Dichloropmpene ND LO 0.005 cis-l,3-Dichloro ro ene ND 1.0 0.005 <br /> ' <br /> trans-l,3-Dichloro ene ND 1.0 0.005 Diiso ro 1 ether DIPE ND 1.0 0.005 <br /> Eth lbenzene ND 1.0 0.005 Ethyl tert-butyl ether ETBE ND 1.0 0.005 <br /> Freon 113 ND 1.0 0.1 Hexachlombutadiene ND LO 0.005 <br /> H=wItloroethane ND 1.0 0.005 2-Hexanone ND 1.0 0.005 <br /> Esopropylbenzene ND 1.0 0.005 4-1so ro1 toluene ND 1.0 0.005 <br /> Meth I-t-bu I ether E ND 1.0 0.005 Methylene chloride ND 1.0 0.005 <br /> 4-Meth I-2- entanone IBK ND 1.0 0.005 Na hthalme ND 1.0 1 0.005 <br /> Nitrobenzene ND 1.0 0.1 1 n-Pro1 benzene ND 1.0 0.005 <br /> Styrene ND 1.0 0.005 1,1,1,2-Tetrachloroethane ND 1.0 0.005 <br /> 1,1,2,2-Tetrachloroethane ND 1.0 0.005 Tetrachloroethene ND 1.0 0.005 <br /> Toluene ND 1.0 0.005 1,2,3-Trichlorobenzene ND 1.0 0.005 <br /> 1,2,4-Trichlorobenzene ND LO 0.005 1,1,1-Trichloroethane ND 1.0 0.005 <br /> 1,1,2-Trichloroethane ND 1.0 0.005 Trichloroethene ND 1.0 0.005 <br /> Trichlorofluoromethane ND 1.0 0.005 1,2,3-Trlchloro ro ane ND 1.0 0.005 <br /> 1,2,4-Trimeth Ibenzene ND 1.0 0.005 1,3,5-Trimeth Ibenzene ND LO 0.005 <br /> Vinyl Chloride ND 1 1.0 1 0.005 Xylenes I ND 1 1.0 1 0.005 <br /> Surrogate Recoveries(%) <br /> %Ssl; 83 %SS2: 109 <br /> %SS3: 107 <br /> Comments: <br /> •water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> ' h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to high <br /> organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight;m) <br /> Ireporting limit raised due to insufficient sample amount;n results are reported on a dry weight basis; see attached narrative. <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />