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� �'� aro. i s �� f,�nm� �-� _�... �f.i� '.` �+'"rt1 ��'���• 'rte."� � �Y' �'-�, <br /> E <br /> F. Ice the sample vials immediately and keep them iced <br /> through shipr:ent. <br /> L. Fill Gut chain-of-custody form. Sop 11 given major <br /> details. Make sure sample requests is fcor-proper <br /> anal;sis t_+.►pe. <br /> M. . Shipping of hazardous materials (methanol.) requires <br /> special documents from Federal Express and UPS. <br /> Briefly you will need to add following to outside of <br /> package and on documents: <br /> 1. Flammable liquid label (some will come from lab <br /> with the vials) . <br /> 2. "UH1230 methyl alcohol". <br /> 3. For UPS, a "Hazardous Material" label. <br /> - N. Ship overnight delivery to the lab. If dry ice is <br /> _. available, up to 5 pounds per package can be sent via <br /> Federal Express by simply writing "ORM-A dry ice, <br /> - pounds, for research" on outside of package and on <br /> shipping document. UPS does not accept dry-ice <br /> shipments. <br /> 5. Good sampling practice would include preparing one out of <br /> five samples to be preparedin uplicatesfforor tanalysis.he following <br /> These four out of twenty s <br /> will purposes: <br /> A. One in every twenty samples should be analyzed as a <br /> field replicate to evaluate the precision of the <br /> sampling technicque. A minimum of one sample per <br /> data set is suggested. <br /> B. An additional one in twenty samples should be selected <br /> w by sampler to be prepared in duplicate as alternative <br /> to Step (A) . Choose a different soil type if <br /> available. <br /> C. The lab does spiking with reference materials fo:r <br /> internal Quality Control (QC) iso additionallllyia minimum <br /> of two in twenty samples need to be prep <br /> ared duplicate. <br /> � ,� GkUI'\li0'ATF:H <br /> is7 <br />