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Lancaster <br /> WLaboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster,PA 17605-2425•717 656 2300 Fax 717-656-2681•www lanaasterlabs corn <br /> Page 3 of 3 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 889747 <br /> Reported 04/03/04 at 07 25 PM <br /> LCSD 94 Surrogate Qual,Lty Control. <br /> MS 102 <br /> MSD 102 <br /> Limits 57-146 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDB <br /> Batch number P040901AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 9242261 99 94 98 95 <br /> 4242262 98 93 98 96 <br /> 4242263 100 93 98 93 <br /> 4242264 96 96 98 92 <br /> 4242265 100 95 98 94 <br /> 4242266 99 94 98 93 <br /> 4242267 98 93 98 94 <br /> 4242268 100 95 97 92 <br /> 4242269 100 93 97 92 <br /> Blank 98 94 97 93 <br /> LCS 99 94 98 95 <br /> MS 100 94 98 95 <br /> MSD 98 94 98 93 <br /> mita 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+MTBE by 8260B <br /> Batch number P040902AA <br /> Dzbromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4242260 102 97 95 94 <br /> Blank 102 98 95 95 <br /> LCS 101 97 97 94 <br /> MS 102 96 96 94 <br /> MSD 101 97 96 94 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name 8260 Master Scan (water) <br /> Batch number P040911AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> Blank 100 96 98 93 <br /> LCS 100 95 98 94 <br /> MS 98 96 97 94 <br /> MSD 99 95 97 94 <br /> Limits 81-120 82-112 85-112 83-113 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> } The background result was more than four times the spike added <br />