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6 <br /> Quality Assurance Plan <br /> The procedures to be followed in sample collection, identifica- <br /> tion, and handling at the site are described below. The analytical <br /> quality assurance program is also discussed. <br /> Sample Collection and Handling <br /> Proper collection and handling are essential in ensuring the <br /> quality of the sample. All samples will be collected by experienced <br /> field personnel. The samples will be collected in suitable <br /> containers which have been precleaned at the laboratory. The <br /> containers will be clearly marked and dated for identification. All <br /> samples will be cooled and stored for analysis no longer than the <br /> maximum allowable holding time. <br /> Sample Identification and Chain-of- <br /> Custody Procedures <br /> Sample identification and chain-of-custody procedures ensure <br /> sample integrity and document sample possession from the time of <br /> collection to its ultimate disposal. Each sample container submitted <br /> for analysis will have a label affixed to identify the job number, <br /> sampler , date and time of sample collection, and a sample number <br /> unique to that sample. This informatiion, in addition to a <br /> description of the sample, field measurements made, sampling <br /> methodology, names of on-site personnel, and any other pertinent <br /> field observations, will be recorded on the boring log or in the <br /> field records. <br /> A chain-of-custody card (Figure 3) will be used to record <br /> possession of the sample from time of collection to its arrival at <br /> the laboratory. The sample control officer at the laboratory will <br /> verify sample integrity and confirm that it was collected in the <br /> proper container , preserved correctly, and that there is an adequate <br /> volume for analysis. If these conditions are met, the sample will be <br /> assigned a unique log number for identification throughout analysis <br /> and reporting. The log number will be recorded on the chain-of- <br /> custody card and in the legally required log book Brown and Caldwell <br /> maintains at the laboratory. The sample description, date received, <br /> client' s name, and any other relevant information will also be <br /> recorded. <br /> Laboratory Anaytical Quality Assurance <br /> In addition to routine calibration of the instruments with <br /> standards and blanks, the analyst is required to run duplicates and <br /> spikes on 10 percent of the analyses to ensure an added measure of <br /> precision and accuracy. Accuracy is also verified through the <br /> following: <br />