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VERMCAnON LABORATORY <br /> . ANAILPSIS <br /> a TANK TAMC •TPH=G TPH-D STX & E CL KCTOTAL <br /> CONTENTS 8015 MT3E =METALS <br /> Y 8260 801 8020 3010- LEAD TBA, IC:-IP/ PCB <br /> 8260 8260 824p 74 <br /> y0- DIPS, AES or 8270 <br /> 8080 <br /> 11421 E'TBE. AA &a g z <br /> TAME f. <br /> I 8260 <br /> - f LEADED GAS <br /> i X X <br /> I f <br /> X � X <br /> UNL GAS X <br /> I # X <br /> DIESEL <br /> KEROSEfYE I X X <br /> I UNK FUEL X X X <br /> X J X <br /> PROD. OIL I S <br /> CHLOR. <br /> SOL VaNTs <br /> x <br /> X <br /> NOfvCHLOR <br /> SOLVEN'T'S � X <br /> t <br /> Tk-L wAST>r\ <br /> USED OIL X X X <br /> X } <br /> I ALIanalysis methods are the designatedf X X <br /> E.a A methods described in EPA SW 846, Third E . <br /> SW 846 are specifically noted below. Refe:to the 'SwRC3 LUFT Field Manual i' m °n' Those methods no[ ;quad is <br /> li minimum detection limits for motor vehicle fuel , Appeu i D (3), Tame 3-s on page A20 for l <br /> for Initial Evaluation and Investigation of uST,S- for Board oil to 1-2-3 "Rem <br /> Detection Limits that remain below tl[e;yICL �°� Board Starr Recommendations <br /> minimum detection linuts. # <br /> STI.0 or-Allowable Limit a€the ciintamtsiant in question will be accepted, <br /> however laboratory small utilize the most conservative method. <br /> L--kBORkTORY ANALYSES TE. <br /> � TPI-G cthfINOLOGY: 1 <br /> TPH-D Total Petroleum Hydrocarbon, Gasoline. GC <br /> IFID (5030) go 15 mod or GCIMS $260 l <br /> BTX&E TOW Petroleum Hydrocarbon. Diesel. GCIFM(3550). 8015 mod'or GC;Nj 8260 <br /> CL HC Benzene. Toluene,Xylene&Ethyl Benzene, GCrPID 8070 or GGIMS 8260 <br /> TOTAL L:qD Chlorinated I-lydrocaftn, GCIHSD 8010. GC/MS 8240 <br /> Total lead, AA 74M, AA 7421 or ICP-AES 6010 <br /> i MTBE.TAivZ,DIPE.TBA GCIMS 8260 <br /> METS ICRP or AA Inductively Coupled Plasma Atomic Emission S <br /> i <br /> Metals: Spectrometry 6010 or Atomic Absorption Spectrometry'000. <br /> { pC3 'Cadmium, Clzromi:am III and VF, Lead. Zinc and Nickel. <br /> GC-FID ?OiYchlorinated Biphenyls. GCIMS 8210 or 3080 <br /> Method 3050 Gas Chromatography, Flame Ionization Detection <br /> Method 3540 Acid digestion <br /> Method 3550 soxhlet sample prepatadon <br /> Method 5030 Sonication sample preparation, extraction method <br /> {QA/QC Purge and trap sample preparation <br /> Qualiry AssurancclQt ity Control <br /> Noes: To avoid faire poscolumn <br /> ve detection of benzene, benzene-free solvents are to be <br /> 'Columns; a packed column ma be used � - <br /> Y as a 'first cvt" with 'di Fused'capillary columns are preferred to packed <br /> Q�QC is ol{v wed. R3'"samples or once the hydrotsrbons have been characterized and proper <br /> drinking pier spurt�, EPA recommends that the Sflp series for volatile organic should be used in preference to the 600 ser <br /> ,detection limits are lower and the QA/QC is better, Si es exhibiting any level of hep <br /> P - 1ID recommends holding those samples=ti' S series because the <br /> pawl is indicated. <br /> vY metal contamination may require further analysis. <br /> EH 23 046 (Revised 10/19138) <br /> Page 8 <br />