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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax:925-798-1622 <br />' http:l/www.mccampbell.com E-mail:main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Spingolo Trucking Date Sampled: 10/05/01 <br /> 837 Shaw Road Date Received: 10/09/01 <br />' Stockton, CA 95215 Client Contact:Paul Dotson Date Extracted: 10/09/01 <br /> --r' Client P.O: Date Analyzed: 10/12/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 80447 80448 80450 8045I <br /> Reporting Limit <br /> Client ID P3-15 P3-20 P4-15 P4-20 <br />' Matrix S S S S 5 w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND ND 5.0 1.0 <br />' Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 5.0 1.0 <br /> l <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> ie <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br />' tert-Butanol ND ND ND ND 25 5.0 <br />' Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> i <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 110 111 110 107 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-'5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 DN&_'Edward Hamilton,Lab Director <br />