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r - " <br /> tical, Inc. 1534 Willow pass Road,Pittsburg,CA 94565-1701 <br /> McCampbell Analy <br /> } IWeb:www.mccampbcll.com E•rnail:main rr mccampbell.can <br /> "WhenOualityCounts" Telephone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Soil OC Matrix: Soil SatchiD: 37577 WorkOrder: 0808447 <br /> FFA Method SW8015C, Extraction SW3550C Spiked Sample ID: NIA <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> . <br /> mg/Kg mglKg %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS 1 MSD RPD LCSILCSD RPD <br /> TPH-Diesel(C10-C23) NIA 20 NIA N/A NIA 96.8 99.9 3.10 NIA N/A 70- 130 30 <br /> %SS: NIA 50 NIA NIA NIA 105 1 108 2.99 1 NIA NIA 70- 130 30 <br /> All target compounds in the Method Blank-of this extraction batch were ND less than the method RI,with the following exceptions: <br /> NONE <br /> BATCH 37577 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0808447-001A 08!13108 7:45 AM 08/15/08 08/15/08 11:29 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)I(Amount Spiked);RPD=100'(MS- MSD)I((MS+MSD)12). <br /> MS I MSD spike recoveries and I or%RPD may tall outside of laboratory acceptance criteria due to one or more of the following reasons;a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> NIA=net enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS FLAP Certification L644 QA/QC Officer <br />