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Page 15 of 21 <br /> !!science <br /> =nvironmental Quality Control - LCSILCS DuplicateZZ , <br /> AN aboratories, Inc. <br /> Shell Oil Pipeline Company LP Date Received: NIA <br /> P.O- Box 2648 Work Order No: 08-10-1847 <br /> Houston, TX 77252-2648 Preparation: EPA 5030B <br /> Method: EPA 82606 <br /> Project: 25705 Patterson Pass Rd., Tracy, CA <br /> Date Date LCSILCSD Batch <br /> Quality Control Sample ID Matrix Instrument Prepared Analyzed Number <br /> 099-12-796-425. Solid GCIMS XX 10128108 10128/08 081028L02 <br /> Parameter LCS%REG LCSD%REC %REC CL ME CL RPD RPD CL Qualifiers <br /> Benzene 104 104 84114 79-119 0 0-7 <br /> Carbon Tetrachloride 110 108 66-132 55-143 2 0-12 <br /> Chlorobenzene 102 102 87-111 83-115 0 0-7 <br /> 1,2-Dibromoethane 107 106 80-120 73-127 1 0-20 <br /> 1,2-Dichlorobenzene 103 102 79.115 73-121 1 0-8 <br /> 1,1-Dichloroethene 84 80 73-121 65-129 5 0-12 <br /> Ethylbenzene 104 104 80-120 73-127 1 0-20 <br /> Toluene 104 103 78-114 72-120 1 0-7 <br /> Trichloroethene 103 103 84-114 79-119 0 0-8 <br /> Vinyl Chloride 86 84 63-129 52-140 1 0-15 <br /> Methyl-t-Butyl Ether(MTBE) 121 119 77-125 69-133 1 0-11 <br /> Tert-Butyl Alcohol(TBA) 131 135 47-137 32-152 3 0-27 <br /> Di isopropyl Ether(DI PE) 108 107 76-130 67-139 1 0-8 <br /> Ethyl-t-Butyl Ether(ET BE) 118 115 76-124 68-132 2 0-12 <br /> Tert-Amyl-Methyl Ether(TAME) 117 114 82-118 76-124 3 0-11 <br /> Ethanol 75 65 59-131 47-143 14 0-21 <br /> Total number of LCS compounds: 16 <br /> Total number of ME compounds: 0 <br /> Total number of ME compounds allowed: 1 <br /> LCS ME CL validation result: Pass <br /> RPD-Relative Percent Difference, CL-Control Limit <br /> W/k <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL:(714)895-5494 . FAX: (714)894-7501 <br />