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' Appendix D.1:Data Usability Summary <br /> (0.013 gg/L), and pyrene(0.011 µg/L) in this equipment rinsate blank. In addition,equipment blank <br /> QA-R-070312 also had detected amounts of phenanthrene(0.013 gg/L), anthracene (0.010 µg/L), <br /> pyrene(0.010µg/L), and acenaphthylene(0.015 pg/L). The presence of these analytes in the equipment <br /> rinsate may indicate that the decontamination procedure was not adequately performed or there was a <br /> ' source of introduced contamination to the samples. Consequently,these samples were qualified E. <br /> Chain-Of-Custody Forms <br /> ' Sample analytical results were evaluated for agreement with the chain-of-custody form. Based on the <br /> evaluation, all samples were received at the lab in the appropriate containers and in good condition with <br /> the chain-of-custody form filled out properly. <br /> ' Preservation and Holding Times <br /> Samples were preserved in the field as appropriate, were received at the laboratory within the acceptance <br /> temperature criterion of 4±2 °C, and sample preservations—when required by the analysis—were less <br /> than the acceptance pH limit of 2. The samples were prepared and analyzed within specified holding <br /> times. <br /> ' Reporting Limits <br /> Data reported for this sampling event were reported within the laboratory MDLs. The MDL represents <br /> the lowest concentration point where an analyte can be positively identified,but the quantitation is an <br /> ' estimate. The LOQ is the lowest concentration of an analyte in a sample that the laboratory can report <br /> with precision and accuracy. Analytes that were reported between the MDL and LOQ for this data set <br /> were qualified J as estimates. <br /> Laboratory Fuel Notes for TPH-d Analysis <br /> The laboratory made several notes on the observed chromatogram patterns for groundwater samples <br /> ' analyzed for TPHd. Groundwater samples CPL-087-W-070313, SB-37-W-070313, SB-41-W-070312, <br /> SB-40-W-070312, QA-R-070312, and SB-39-W-070312 had observed TPHd patterns that include#2 fuel <br /> diesel and an additional pattern that elutes later in the diesel-carbon range. <br /> Completeness <br /> Completeness is defined as the number of valid results (i.e., those not rejected) divided by the total <br /> number rejected. Evaluation of the data against the QC objectives indicated that the percentages of valid <br /> ' data for each method are 100 percent, with no data rejected for this investigation. <br /> Comparability <br /> The data evaluation determined that the data are comparable with other laboratory data for similar <br /> samples and sample conditions. The sample collection techniques,EPA test methods, detection limits, <br /> analytical laboratory, units of measure,and sample preparation procedures were selected to ensure data <br /> ' comparability on this project. <br /> SUMMARY <br /> SAIC's evaluation concluded that all analytical data are usable as qualified for the purpose of determining <br /> chemical concentrations in soil and groundwater at the Tracy Byron Road site in Tracy, California. <br /> Data associated with SDGs for this sampling event were qualified for LCS/LCSD recoveries,MS/MSD <br /> recoveries, surrogate recoveries, field blank contamination, and results reported between the laboratory <br /> MDL and LOQ. Qualified data with applicable reason codes are shown in Table D-1. <br /> Analytical data collected in support of this investigation are considered precise, accurate,representative, <br /> ' complete, and comparable, and they may be used for their intended purposes unless noted otherwise. <br /> ' Page D.1-4 <br /> Jr: ` <br /> From Science to <br /> Solutions <br />