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QUALITY ASSURANCE REPORT <br /> ZY MIPA <br /> MATRIX SPIKE DUPLICATE RESULTS <br /> Client: Jeff Willett Lab Number: 24281-1 MSD <br /> Condor Earth Technologies, Inc. Collected: 06/20/01 <br /> 188 Frank West Circle, Ste. I Received: 06/22/01 <br /> Stockton, CA 95206 Matrix: Soil <br /> Project: Chevron Pipeline Sample Description: <br /> 2496J 1-GP108-1 1.5' <br /> Project Number: 2496.11 Analyzed: 06/26/01 <br /> Collected by: JP Method: See Below <br /> CONSTITUENT Amount Spiked Amount Recovered Percent Relative Percent <br /> mg/kg mg/kg Recovery Difference* <br /> J TOTAL PETROLEUM HYDROCARBONS <br /> Total Petroleum Hydrocarbons (C10-C34) 160. 131. 74 17 <br /> Percent Surrogate Recovery 84 <br /> ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717 <br /> *Relative Percent Difference of the spike and spike duplicate <br /> Note: Analyzed by GC/MS Combination. <br /> Note: Extracted by EPA 3550 on 06/26/01. <br /> Note: Analytical range is C10-C40. <br /> Note: Spiked with crude oil. <br /> Submitted by, <br /> ZymaX envirotechnology, inc. <br /> SS3052 <br /> - MSD #5 <br /> SS3052m.xls �`ichael Ng <br /> MN/jdm/dz/ss/pf Assistant Lab Director <br /> 805.544.4696 <br /> -Son Luis n;,�spo CA 934n'. <br /> %AAAAA/7vrnaXl ISa rTnm iox 805.544.8226 <br />