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QUALITY ASSURANCE REPORT <br /> ZYMAXSPIKE DUPLICATE RESULTS <br /> Client: Lab Number: QSD SA2293 <br /> ZymaX envirotechnology, inc. Collected: <br /> 71 Zaca Lane, Suite 110 Received: <br /> San Luis Obispo, CA 93401 Matrix: Aqueous <br /> Project: Sample Description: <br /> Quality Assurance Spike Duplicate <br /> Project Number: Analyzed: 06/30/01 <br /> Collected by: Method: See Below <br /> CONSTITUENT Amount Spiked Amount Recovered Percent Relative Percent <br /> ug/L ug/L Recovery Difference* <br /> TOTAL PETROLEUM HYDROCARBONS SILICA GEL <br /> Total Petroleum Hydrocarbons (C10-C24) 1000. 469. 47 28 <br /> r <br /> Percent Surrogate Recovery 95 <br /> ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717 <br /> *Relative Percent Difference of the spike and spike duplicate <br /> Note: Analyzed by EPA 8270 and GC/MS Combination. <br /> Note: Extracted by EPA 3510 on 06/20/01. <br /> e Note: Cleanup performed on extract by EPA 3630 (Silica Gel) on 06/28/01. <br /> Note: Analytical range is C10-C40. <br /> Alote: Spiked with diesel fuel. <br /> Submitted by, <br /> ZymaX envirotechnology, inc. <br /> SA2293 <br /> MSD #9 <br /> SA2293s.xls Michael Ng <br /> MN/jdm/dz/yl Assistant Lab Director <br /> 805.544.4696 --— —-- 71 Zara Lone <br /> Son Luis Obispo CA 93401 <br /> www.ZymaXusa.com fox 805.544.8226 <br />