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*Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> ' (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: <br /> 09-Dec-04 OC Summary Report Work Order: <br /> 04120104 <br /> Method Blank Type MBLK Test Code: EPA Method SW8015 <br /> File ID: Batch ID:11235 Analysis Date: 12/02/2004 10:49 <br /> Sample ID: MBLK-11235 Units : mg/Kg Run ID:' FID_1_041202A Prep Date: 12/02/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-E(Diesel) ND 1 <br /> TPH-E(Oil) ND 10 <br /> ' Laboratory Control Spike Type LCS Test Code: EPA Method SW8015 <br /> File ID: Batch ID:11235 Analysis Date: 12/02/2004 10:18 <br /> ' Sample ID: LCS-11235 Units: mg/Kg Run ID:FID_1_041202A Prep Date: 12/02/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-E(Diesel) 124 10 100 124 44 148 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015 <br /> File ID: Batch ID:11235 Analysis Date: 12/03/2004 09:39 <br /> Sample ID: 04120201-01AMS Units: mg/Kg Run ID:FID_1_041202A Prep Date: 12/02/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qua] <br /> TPH-E(Diesel) 401 10 100 0 401 44 153 M53 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015 <br /> ' File ID: Batch ID:11235 Analysis Date: 12/03/2004 11:03 <br /> Sample ID: 04120201-01AMSD Units: mg/Kg Run ID:FID_1_041202A Prep Date: 12/02/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qua] <br /> TPH-E(Diesel) 431 10 100 0 431 44 153 401.4 7.2(49) M53 <br /> ' Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> ' M53=Martix spike recovery was above laboratory acceptance limits and is likely due to the presence of primarily heavy-end hydrocarbons(C 10-C40)that elute out <br /> in both the Diesel and Oil ranges. <br /> 1 <br />