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GeoAnalytical Laboratories, Sc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (2091.-572-0916 <br /> Report# Q338-05 <br /> CERTIFICATE OF ANALYSIS L 11' Date: 12/09/04 <br /> Date;Reed: 12/03/04 <br /> Thorpe Oil Date 4Started;)0(fJJ 2/07/04 <br /> PO Box 357 Project: 216 N. California Street Date Completed:l2/08/04 <br /> Lodi CA 95241 f` <br /> fDate Sampled: 12%03/04 <br /> PO# Time. •` 1:35pm - <br /> Sample ID: Stockpile 1, 2 Sampler : O.Sanchez(Geo) <br /> Lab ID: Q201813,Q201814 <br /> Method RL Analyte Results Units <br /> 8260B 5.0 Benzene ND µg/Kg <br /> 5.0 Toluene ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 10 Methyl tert-butyl ether(MTBE) ND <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Arrant Rec. %Recovery OC Limit% <br /> 1,2-Dichloroethane-d4 20 21.9 109.5 66-133 <br /> 2-Bromo-l-chloropropane 20 22.1 110.5 63-139 <br /> 4-Bromofluorobenzene 20 19.7 98.5 64-136 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 2585 Laboratory Director <br />