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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H4120803 Date: 12/17/2004 Page: 2 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 2111 Method: 8280FA <br /> Prep Meth: SW5030B <br /> Field ID: CPT7 30FT Lab Samp lD: 7611-1S <br /> Descr/Location: CPT7 Recd Date: 12/08/2004 <br /> Sample Date: 12/07/2004 Prep Date: 12/09/2004 <br /> Sample Time: 1140 Analysis Date: 12110/2004 <br /> Matrix: Soil QC Batch: VSMS-0094 <br /> Basis: Wet Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methwert-butyl ether(MTBE) 1.4 10. PQL ND UG/KG i <br /> Ethyl ted-butyl ether(ETBE) Q10 10. PQL ND UG/KG 1 <br /> tert-Amyl methyl ether(TAME) 0.13 10. PQL ND UG/KG 1 <br /> DI-Isopropyl ether(DIPS) Q20 10. PQL ND UG/KG 1 <br /> ter-Butyl alcohol (TBA) 7.0 800. PQL ND UG/KG 1 <br /> 1,2 Dichlorooethane 0.23 10. PQL ND UG/KG' 1 <br /> 1 2-Dibromoethane 0.39 10. PQL ND UG/KG 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> SMSA 83.9% 1 <br /> Toluene-d8 1 <br /> 87.39b <br /> 1,2-Dichloroethan"4 70130 SMSA <br /> i <br /> Date: <br /> Approved by: <br />