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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H4061408 Date: 06/25/2004 Page: 4 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Feel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-2 Lab Samp ID: 7059-3W <br /> Descr/Location: MW-2 Recd Date: 06/15/2004 <br /> Sample Date: 06/11/2004 Prep Date: 06/23/2004 <br /> Sample Time: 1200 Analysis Date: 06/23/2004 <br /> Matrix: Water OC Batch: VWMS-6234 <br /> Basis: Not Filtered Notes: DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 289 5. MRL 59L UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 0.840 5. MRL ND UG/L 10 <br /> tert-Amyl methyl ether(TAME) 0.670 5. MRL ND UG/L 10 <br /> Di-isopropyl ether(DIPS) 1.55 5. MRL ND UG/L 10 <br /> tert-Butyl alcohol (TBA) 87.9 200. MRL ND UG/L 10 <br /> 1,2-Dichloroethane 0.810 5. MRL 6Q UG/L 10 <br /> 1,2-Dibromoethane 0.920 5. MRL 7.0 UG/L 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 63.132 SLSA 85.5% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 88.2% 1 <br /> DF: Reporting limits elevated due to matrix interferences <br /> Approved by: 1L ^ T Date: LQ ,�h7 _ <br />