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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No.: H4061408 Date: 06/25/2004 Page: 6 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-3R Lab Samp ID: 7059-5W <br /> Descr/Location: MW-3R Rec'd Date: 06/15/2004 <br /> Sample Date: 06/11/2004 Prep Date: 06/23/2004 <br /> Sample Time: 1105 Analysis Date: 06/23/2004 <br /> Matrix: Water QC Batch: VWMS-6234 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.289 0.5 MRL 1.6 UG/L 1 <br /> Ethyl tert-butyl ether(ETRE) 0.084 0.5 MRL ND UG/L 1 <br /> ter#-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.155 0.5 MRL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 8.79 20. MRL ND UG/L 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL 1.5 UG/L 1 <br /> 1,2-Dibromoethane 0.092 0.5 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 53-132 SLSA 105% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 94.30 1 <br /> Approved r Date: 6� <br /> taN by: - <br />