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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H4032502 Date: 04/02/2004 Page: 11 <br /> Project Name: OILIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Mehr: SW5030B <br /> Field ID: MW-88 Lab Samp ID: 6797-9W <br /> Descr/Location: MW-8S Recd Date: 03/25/2004 <br /> Sample Date: 03/23/2004 Prep Date: 03/31/2004 <br /> Sample Time: 0745 Analysis Date: 03/31/2004 <br /> Matrix: Water QC Batch: VWMS-3314 <br /> Basis: Not Filtered Notes: DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.578 1. MRL ND UG/L 2 <br /> Ethyl tert-butyl ether(ETRE) 0.168 1. MRL ND UG/L 2 <br /> tert-Amyl methyl ether(TAME) 0.134 1. MRL ND UG/L 2 <br /> Di-isopropyl ether(DlPE) 0.310 1. MRL 1.7 UG/L 2 <br /> tent-Butyl alcohol (TBA) 17.6 40. MRL ND UG/L 2 <br /> 1,2-Dichloroethane 0.81 5. MRL 170. UG/L 10 <br /> 1,2-Dibromoethane 0.184 1. MRL ND UG/L 2 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 116°x6 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 99.6% 1 <br /> DF: Reporting limits elevated due to matrix interferences <br /> Vow <br /> Approved by:- - ._ -.- -_ Date: <br />