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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3062702 Date: 07/10/2003 Page: 2 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 2ND QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-1 Lab Samp ID: 6858-1W <br /> Descr/Location: MWA Rec'd Date: 06/27/2003 <br /> Sample Date: 06/25/2003 Prep Date: 07/02/2003 <br /> Sample Time: 1345 Analysis Date: 07/02/2003 <br /> Matrix: Water QC Batch: VWMS-7023 <br /> Basis: Not Filtered Notes: DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 44.45 25, MRL 800. UG/L 50 <br /> Ethyl tert-butyl ether(ETBE) 4.2 25. MRL ND UG/L 50 <br /> tert-Amyl methyl Ether(TAME) 3.35 25. MRL. ND UG/L 50 <br /> Di4sopropyl ether(DIPE) 7.75 25. MRL ND UG/L 50 <br /> tent-Butyl alcohol (TBA) 439.5 1000. MRL. ND UG/L 50 <br /> 1,2-Dichloroethane 4.05 25. MRL 290. UG/L 50 <br /> 1,2-Dibromoethane 4.6 25. MRL 160. UG/L 50 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 111% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 96.8% 1 <br /> qW DF: Reporting limits elevated due to matrix interferences <br /> Approved by: % �' Date: I lIJ <br />