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Castle Analytical Laboratory, Atwater, CA <br /> ab Report No.: H3062702 Date: 07/10/2003 Page: 7 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 2ND QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-3R Lab Samp ID: 5858-6W <br /> Descr/Location: MW-3R Rec'd Date: 06/27/2003 <br /> Sample Date: 06/25/2003 Prep Date: 07/02/2003 <br /> Sample Time: 1658 Analysis Date: 07/02/2003 <br /> Matrix: Water QC Batch: VWMS-7023 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-telt-butyl ether(MTBE) 0.289 0.5 MRL 0.64 UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0.084 0.5 MRL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0.155 0.5 MRL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 8.79 20. MRL ND UGIL 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL 0.67 UG1L 1 <br /> 1,2-Dibromoethane 0.092 0.5 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 115% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 112% 1 <br /> r <br /> Approved by: N Date: l a <br />