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V <br /> Castle Analytical Laboratory,Atwater, CA <br /> ab Report No.: H3062702 Date: 07/10/2003 Page: 13 <br /> oJect Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 2ND QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-9 Lab Samp ID: 5858-12W <br /> Descr/Location: MW-9 Recd Date: 06/27/2003 <br /> Sample Date: 06/25/2003 Prep Date: 07/02/2003 <br /> Sample Time: 1800 Analysis Date: 07/02/2003 <br /> Matrix: Water QC Batch: VWMS-7023 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.289 0.5 MRL ND UG/L 1 <br /> Ethyl tert-butyl ether (ETBE) 0.084 0.5 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.155 0.5 MRL ND UG/L 1 <br /> tert-Butyl alcohol (CBA) 8.79 20. MRL ND UGIL 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 0.092 0.5 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 104% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 118% 1 <br /> Approved by: Date: <br />