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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3040102 Date: 04/09/2003 Page: 14 <br /> Project Name: OLVAREZ PROPERTY Analysis: Volatile Organic Compounds by GCIMS Fuel <br /> Project No: 1 ST QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-1 Lab Samp 10: 33857-001 <br /> Descr/Location: MWA Recd Date: 04/01/2003 <br /> Sample Date: 03/28/2003 Prep Date: 04/03/2003 <br /> Sample Time: 1210 Analysis Date: 04/03/2003 <br /> Matrix: Water QC Batch: WMS110008 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert•butyl ether(MTBE) 7.5 25. PQL 140Q UG/L 25 <br /> Ethyl tert-butyl ether(ETBE) 12.5 125. PQL ND UG/L 25 <br /> tent-Amyl methyl ether(TAME) 7.5 125. PQL ND UG/L 25 <br /> Di-isopropyl ether(DIPS) 12.5 125. PQL ND UG/L 25 <br /> tert-Butyl alcohol (TBA) 115. 250. PQL 29Q UG/L 25 <br /> 1,2-Dichloroethane 7.5 125. PQL 36Q UG/L 25 <br /> 1,2-Dibromoethane 1 12.5 125. PQL 15Q UG/L 25 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 91.7% 1 <br /> Toluene-d8 77-150 SMEA 84.4% 1 <br /> Dibromofluoromethane 57-156 SMEA 94.2% 1 <br /> M <br /> uate: <br /> Approves Dy: C <br />