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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3040102 Date: 04/09/2003 Page: 23 <br /> Project Name: OLVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 1 ST QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-8S Lab Samp ID: 33857-009 <br /> Descr/Location: MW-8S Recd Date: 04/01/2003 <br /> Sample Date: 03/28/2003 Prep Date: 04/07/2003 <br /> Sample Time: 1300 Analysis Date: 04/07/2003 <br /> Matrix: Water QC Batch: WMS110015 <br /> Basis: Not Filtered Notes: BH <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyi-tert-butyl ether(MTBE) 3. 10. PQL ND UGIL 10 <br /> Ethyl ter#-butyl ether(ETBE) 5. 50. PQL ND UGIL 10 <br /> tert-Amyl methyl ether(TAME) 3. 50. PQL ND UGIL 10 <br /> Di-isopropyl ether(DIPE) S. 50. PQL ND UGIL 10 <br /> tert-Butyl alcohol (TBA) 46. 100. PQL ND UGIL 10 <br /> 1,2-Dichloroethane 3. 50. PQL 68 UGIL 10 <br /> 1,2-Dibromoethane 5. 50. PQL ND UGIL. 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 103.0% 1 <br /> Toluene-d8 77-150 SMEA 102.0% 1 <br /> Dibromofluoromethane 57-156 SMEA 102.0% 1 <br /> BH: Reporting limits raised due to high level of non-target analytes <br /> Approvea Dy: to _ uate: �t j 3 <br />