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Entech Analytical labs, Inc. <br /> • 3334 Victor Court • Santa Clara, CA 95054 • (408) 588-0200 Fax (408) 588-0201 <br /> Sherwood Labs Corporation Date: 04/05/01 <br /> P.O.Box 937 Date Received: 3/26/01 <br /> Project Name: Olivarez <br /> Hilmar,CA 95324 Project Number: <br /> Attn: Vicki Hubis P.O.Number: Olivarez <br /> Sampled By: Client <br /> Certified Analytical Report <br /> Order ID: 24930 Lab Sample ID: 24930-011 Client Sample ID: MW#8 @ 75' <br /> Sample Time: Sample Date: 3/21/01 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Analysis Date QC Batch ID Method <br /> Diisopropyl Ether ND 1 5 5 µg/Kg 4/1/01 SMS2010331 EPA 8260E <br /> Ethyl-t-butyl Ether ND 1 5 5 µg/Kg 4/1/01 SMS2010331 EPA 8260B <br /> Methyl-t-butyl Ether ND 1 5 5 pg/Kg 4/l/01 SMS2010331 EPA 8260B <br /> tent-Amyl Methyl Ether ND 1 5 5 µg/Kg 4/1/01 SMS2010331 EPA 8260B <br /> tert-Butanol ND 1 20 20 pg/Kg 4/l/01 SMS2010331 EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits(%} <br /> 4-Bromofluorobenzene 94 56 - 131 <br /> Dibromofluoromethane 159 65 - 135 <br /> Toluene-d8 96 65 - 135 <br /> Comment: Surrogate recovery out of control limits due to matrix interference. <br /> *—Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Entech Analytical Labs,Inc.(CA ELAP#2346) <br /> Mich . Anderson, Laboratory Director <br /> Environmental Analysis Since 7983 <br />