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110 Second Avenue uth,##D7,Pacheco,CA 94553-5560 <br /> MCCANTBELL ANALYTICAL INC. Telephone: 925-798-I620 Fax:925-798-1622 <br /> hftP://www-mr&arnPbell wrn E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Emil's Liquors Date Sampled: 01/28/99 <br /> 4005 North Wilson Way Date Received: 01/30/99 <br /> Stockton, CA 95205 Client Contact: Gary Dickenson Date Extracted: 02/01/99 <br /> Client P.O: Date Analyzed: 02/02-02/08/99 <br /> Diesel Range(CIO-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ %Recovery <br /> Surrogate <br /> 02594 SB-1-1 I' S ND 96 <br /> 02597 SB-1-26.5' S ND 98 <br /> 02598 SB-1-31' S ND 94 <br /> 02599 SP-7 S 1.2,b 96 <br /> 02600 SP-6 S 3.5,b,g gg <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> water and vapor samples are reported in ug/L.,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC!SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel (?)• f) <br /> one to a few isolated peaks present;g)oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than--5 vol.%sediment. <br /> DHS Certification No. 1644 //l Edward Hamilton, Lab Director <br />