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I t i i t l <br /> f4s` <br /> CLIENT: Condor Earth Technologies <br /> Work order: 076516 ANALYTICAL QC SUMMARY REPORT <br /> h a Project: Proposed Women/Children Center,4634 <br /> TestCode: 8081 S <br /> M Sample ID: 076538-004AMS SampType: MS TestCode: 8081_S Units: pg/Kg Prep Date: 5/20/2005 Run ID: GC10_050521A <br /> N Client ID: ZZZZZ Batch ID: 22780 TestNo: EPA 8081A (EPA 3550B) Analysis Date: 5/21/2005 SegNo: 736361 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> 4,4"-DDT 9617 2.0 16.65 5186 26600 48 150 0 0 SE <br /> Aldrin 22.65 1.0 16.65 0 136 78 136 0 0 S <br /> w Dieldrin 25.33 2.0 16.65 0 152 72 136 0 0 S <br /> N Endrin 27.02 2.0 16.65 0 162 74 150 0 0 S f <br /> - i <br /> gamma-BHC 23.64 1.0 16.65 0 142 76 138 0 0 S <br /> Heptachlor 23.76 1.0 16.65 0 143 71 149 0 0 <br /> Sample ID: 076524-020AMSD SampType: MSD TestCode: 8081 S Units: pg/Kg Prep Date: 5/19/2005 Run ID: GC5_050519A <br /> a - <br /> c Client ID: 7777 Batch ID: 22768 TestNo: EPA 8081A (EPA 3550B) Analysis Date: 5/20/2005 SegNo: 734759 <br /> m <br /> S <br /> ti <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> CI' 4,4"-DDT 360.6 2.0 16.65 587.7 -1360 48 150 539.7 39.8 30 SRE <br /> W <br /> a <br /> Aldrin 20.76 1.0 16.65 0 125 78 136 20.56 0.950 30 <br /> Dieldrin 20.77 2.0 16.65 0 125 72 136 20.87 0.473 30 <br /> Endrin 22.2 2.0 16.65 0 133 74 150 22.18 0.0706 30 <br /> n gamma-BHC 21.65 1.0 16.65 0 130 76 138 21.63 0.0947 30 <br /> Y Heptachlor 21.5 1.0 16.65 0 129 71 149 21.3 0.945 30 <br /> O <br /> Sample ID: 076538-004AMSD SampType: MSD TestCode: 8081 S Units: pg/Kg Prep Date: 5/20/2005 Run ID: GC10 050521A <br /> Client ID: 7777 Batch ID: 22780 TestNo: EPA 8081A (EPA 3550B) Analysis Date: 5/21/2005 SegNo: 736362 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> 4,4'-DDT ND 2.0 16.65 5186 -31100 48 150 9617 0 30 S <br /> Aldrin 23.48 1.0 16.65 0 141 78 136 22.65 3.60 30 S <br /> a Dieldrin 23.91 2.0 16.65 0 144 72 136 25.33 5.76 30 S <br /> pEndrin 23.56 2.0 16.65 0 141 74 150 27.02 13.7 30 <br /> c� gamma-BHC 24.45 1.0 16.65 0 147 76 138 23.64 3.33 30 S <br /> Heptachlor 24.6 1.0 16.65 0 148 71 149 23.76 3.46 30 <br /> �n <br /> a <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits DO-Surrogate dilute out <br /> �o J-Analyte detected below quantitation limits B-Analyte detected in the associated Method Blank H-Sample exceeded holding time <br /> R-RPD outside accepted recovery limits Calculations are based on raw values Page 14 of 18 <br /> O <br /> Page 45 of 49 <br />