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3 1 - <br /> ' 14I'N1M(jM VERIFICATION LAIjoltATORY ANALYSIS i <br /> BE METALS PCH <br /> 'TANK 'f ANK TPI-1-0 1711-13 BTX & E L F#C TOTAL MT 8n15 #CA8270 <br /> iI0 LEAD 8020 / 8080 <br /> # CON'T'EN'T'S 8)15 �(}26t01 240 7420APES <br /> ICAPI <br /> $ZG) 8260 7421 AA <br /> 7 <br /> LEADED X X X <br /> OAS ,._-- <br /> __._�_- uNL OAS x --- <br /> X <br /> ----�- <br /> DIESEL X X <br /> KEROSENE x x <br /> ---- � X <br /> UNK FUEL X X X <br /> PROD. OIL X X <br /> CHLOR. X X <br /> SOLVENTS <br /> NONCIILOR x x X <br /> . SOLVENTS <br /> WASTFA X X X <br /> USED nil.. X X X <br /> L I <br /> All analyses methods are designated EPA methods described in EP SW 846,Third Edition. Those ,Tata 3-otrorund <br /> it, SW 846, are specifically noted below. Refer to the SWRCn L t T -24 Manual A{rP <br /> detection limits or motor vehicle fuels (,gasoline and diesel). Refe l0 1-Z-3 `Regional Board Staff Recommendations for <br /> initial Evaluation and Investigation or USI, for The waste and motor oil detection limits. <br /> !)etectlotr IJmiis that remain below the MCI, STIC or er votive m tlowable Limit of the cnntprrrinnnt inn question will be accepted, <br /> 11mre:er laboratory alnoil utilize Ilse moa <br /> LAnoRA'fORY ANALYSES 'f'ERMINOLOOY: C/I;ID (SU3n) 8015 rood or OClMS 8260 <br /> fPit•CI Total Petroleum Hydrocarbon, Gasoline, <br /> i'I'I1 !7 Total Pettoleunn t-lydrocartmn, Diesel, O lD (3550), 8017 mod or GC/MS 8260 <br /> il'1'X A E Benzene, 'Foluene, Xylene & Ethyl Dente e, aCIP117 8020 or GC/MS 8260 <br /> CL 1!C Chlorinalcd I lydrocarbon, OC/1-ISD 80111, OC.JMS 8240 <br /> 'l'U'!'AL LEAD 'Intal lead, AA 7420, AA 7421 or !CP-A 6010 <br /> EUB Ethylene dtbr;imide (DHS-AB t8t)3), O S 8240 (DHS-LUFT) <br /> (W-FID Oas Chromatography, Flame lonirati In etenition <br /> ICAP or AA Inductively Coupled Plasma Atomic Em1 tan Spectrometry 6Ulq or Atomic Absorption <br /> Spectrometry 7000. Metalsr E aduriu Chromium in and Vi, Fend, Zlnc and Nickel. <br /> PCB Polychlorinated Blphenyls, GC/MS 8270, r 8080 <br /> Metiu)d 3050 Acid digestion <br /> Method 3540 Soxhiet sample preparation <br /> Melhotl 3551) Sonication Sample proiaratiott, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quallty Control <br /> Notes: To avoid raise positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns-$ a packed column may be used as a "First cut" with "dirty` samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> I:or Drinking water sources. EPA recommends that the 5(X)series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC Is be ler. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis. PIIS-EMD recommends holding these samples until disposal Is indicated. <br /> Ell23 048 (Rev1sedXxXl3) Page 8 <br /> 2/26/96 <br /> lr, <br />