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QA* Report <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> Sherwood Labs Corporation, Hilmar, CA <br /> Lab Report No H1091702 Date 09/25/2001 Page 10 <br /> QC Batch BWA091901 Protect Name Lab Generated or Non COE Sample <br /> Matrix Water Project No Lab Generated or Non COE Sample <br /> Lab Samp ID BWA091901 Field ID Lab Generated or Non COE Sample <br /> Basis Not Filtered Lab Ref 1D PH1090338Q <br /> Analysis Spike LeSpike Sample S ike Result % Recoveries Acceptance <br /> Analyte Method MS DMS Result MSDMS Units MS DMS RPD % RecCri#eriaRPD <br /> Benzene SW802OF 372 3 72 259 3047 28 B3 UGIL 123 78 8 441 130-70 MEA 30MEP <br /> Ethylbenzene SW8020F 8 7 87 34 1386 1312 UGIL 120 112 6 9 130-70 MEA 30MEP <br /> Gasoline SW8020F 637 637 964 1581 1546 UGIL 969 914 58 130-70 MEA 30MEP <br /> Methyt-tert-butyl ether SW8020F 3464 3464 ND 5749 4955 UG/l. 1661 1434 15 130-70 MEA 30MEP <br /> Toluene SW8020F 31 31 44 4786 4172 UGIL 1381 118 16 130-70 MEA 30MEP <br /> Xylenes SW802OF 487 48 7 120 7160 7506 UGIL 123 130 55 130-70 MEA 30MEP <br /> 4-Bromoftuorobenzene SW8020F 100 100 146. 135 149 PERCENT 1351 149' 99 130-70 SMSA 30SMEP <br /> Chlorobenzene SW802OF 100 100 295 364 331 PERCENT 3641 331! 95 130-70 SMEA 30SMEP <br /> BC Matrix spike out of control,tab control sample within limits <br /> CR QC criteria not met,sample reanatyzed with similar results <br /> DB QA results outside of aoceptance limits due to matrix effects <br />