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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> Fax (209)384-1507 <br /> Foothill Engineering Client Project ID Vogue Cleaners Method EPA 5030/8260 <br /> 8442 Story Ridge Way Reference Number 8664 Instrument ID HP 5972 MS <br /> Antelope,CA 95843 Matrix Water Prepared 10-25-05 <br /> Attn Mike Vlach Analyst S Foster Analyzed 10-25-05 <br /> Reported 11-03-05 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID VWMS-0255 <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Leve[ Spike Limits <br /> u /L u /L u /L %R <br /> COMPOUNDS <br /> t-Bu I Alcohol(t-BA) 20 ND 750 102% 576-163 <br /> Methyl t-butyl ether MTBE 050 ND 250 108% 647-134 <br /> Diiso rol ether DIPS 050 ND 250 104% 582-135 <br /> Ethyl t-Butyl ether ETBE 050 ND 250 105% 650- 132 <br /> t-Ami methyl ether AME 050 ND 250 944% 61 0-139 <br /> 1 2-Dichloroethane(1,2-DCA) 050 ND 250 120% 701 -145 <br /> Ethylene dibromide EDB 050 ND 250 122% 550-156 <br /> 1 1-Dichloroethene 1 1 DCE 050 ND 250 105% 545-154 <br /> Benzene 0 50 ND 250 114% 771 -132 <br /> Trichloroethene CE 050 ND 250 116% 774-118 <br /> Toluene 0 50 ND 2 50 117% 705-130 <br /> Chlorobenzene 050 ND 250 121% 820-125 <br /> Surro ate <br /> Dibromofluoromethane 100 120% 100 106% 667-132 <br /> 1 2-Dichloroethane-d4 100 984% 100 987% 592-135 <br /> Toluene-dB 100 103% 100 108% 62 9-132 <br /> 4-Bromofluorobenzene 100 1 108% 100 104% 697-131 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> u /L %R %R <br /> COMPOUNDS <br /> t-Bu I Alcohol t-BA 750 957% 109% 397-178 12 9% <br /> Methyl t-butyl ether MTBE 250 104% 110% 553-144 599% <br /> Diisopropyl ether DIPS 250 106% 109% 549-135 335% <br /> Ethyl t-ButvI ether ETBE 250 968% 109% 540-136 120% <br /> t-Am I methyl ether AME 250 700% 812% 396-131 126% <br /> 1 2-Dichloroethane 1 2-DCA 250 116% 122% 73 9-147 480% <br /> Ethylene dibromide EDB 250 112% 114% 633-141 213% <br /> 1 1-Dichloroethene 1,1 DCE 250 103% 109% 545-154 604% <br /> Benzene 250 108% 114% 771 -132 5 31% <br /> Trichloroethene TCE 250 107% 119% 774-118 110% <br /> Toluene 250 111% 113% 705-130 168% <br /> Chlorobenzene 250 113% 116% 820-125 242% <br /> Surrogate <br /> Dibromofluoromethans 10 0 110% 111% 667-132 0 723% <br /> 1 2-Dichloroethane-d4 100 102% 105°� 59 2-135 3 29% <br /> Toluene-d8 100 100% 104% 629-132 4 11% <br /> 4-Bromofluorobenzene 100 105% 106% 697-131 1 0 95°k <br /> APPROVED BY ( I�Q" <br /> James C Phillip'41/Laboratory Drrector or <br /> Clan J Cone/L boratory Manager <br />