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Date January 24,2005 <br /> Quarter 4'b Quarter,2004 <br /> APPENDIX B <br /> FIELD AND LABORATORY PROCEDURES <br /> Sampling Procedures <br /> Sampling equipment is thoroughly cleaned prior to the collection of each sample The sampling procedure for each <br /> well includes measuring the water level and checking for the presence of separate-phase hydrocarbons (SPH), using <br /> either an electronic indicator and a clear Teflon® bailer or an oil-water interface probe Wells not containing SPH <br /> are purged of approximately three casing volumes of water (or to dryness) using a submersible pump, centrifugal <br /> pump, gas displacement pump, or bailer The equipment and purging methods used for the current sampling event <br /> are noted on the attached field data sheets During purging, temperature, pH, electrical conductivity, and dissolved <br /> oxygen are monitored in order to document that these parameters are stable prior to collecting samples After <br /> purging, water levels are allowed to partially recover Groundwater samples are collected using a clean disposable <br /> Teflon®bailer,placed into appropriate EPA-approved containers, labeled,logged onto chain-of-custody documents, <br /> and transported on ice to a California state-certified laboratory <br /> Decontamination Procedures <br /> Prior to sampling each well,reels,and pumps will be decontaimnated with a steam cleaner Sensitive equipment such <br /> as the water level sounder are sprayed with a non-phosphate soap and deionized water solution and rinsed with <br /> delonized water All water used for equipment decontamination is collected and contained in a truck-mounted water <br /> tank <br /> iLaboratory Procedures <br /> The groundwater samples are analyzed for the following GRO (gasoline range organics C4 — C12) using EPA <br /> Method 8015B due to capacity issues at the laboratory, BTEX, fuel oxygenates, 1,2-DCA, and EDB using EPA <br /> Method 8260B, and Methanol using EPA Method 8015B The methods of analysis for the groundwater samples are <br /> documented in the Iaboratory analytical report The laboratory analytical report, chain-of-custody documentation, <br /> and field data sheets are presented as Appendix C <br /> Purge and Rinsate Water Disposal <br /> I <br /> Water generated during well sampling and equipment cleaning is pumped into a truck-mounted water tank The <br /> water is transported to the Blaine Tech Services holding facility in Roseville, California, or in the ARCO holding <br /> facility in West Sacramento, California, for temporary storage Dillard Environmental Services then transports the <br /> water to the Altamont Landfill and Resource Recovery Facility in Altamont,California,for disposal <br /> K kWp,oze.,j5 BP ARC04021865Q..tuW004\4 QTR 04\2186 GWMR 4Q04 doe Page B-1 <br />