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Lancaster <br /> 4 Laboratories Analysis Report <br /> Y � <br /> 2425 New H011and Pike PO Box 12425 Lancaster PA 17605 2425•717-856 2300 Fax 717-656-2581•www lancastarlabs com <br /> ' Pagel of 3 <br /> Quality Control Summary <br /> ' Client Name ChevronTexaco Group Number 864230 <br /> Reported 09/02/03 at 04 03 PM <br /> ' Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> al si Name Result ISL Unite "Imc 9RBC Litnity RPD RPD KaX <br /> Batch number 03237A07C Sample number(s) 4107519 <br /> ' TPH-GRO - Waters N ❑ So ug/1 97 107 70-130 10 30 <br /> Batch number 03237A55A Sample number(s) 4107520-4107522 <br /> TPH-GRO - Waters N D 50 ug/l 86 90 70-130 4 30 <br /> ' Batch number 032410017A Sample number(s) 4107519-4107522 <br /> Methanol (by Direct Injection) 590 200 ug/l 116* 78-114 <br /> Batch number N032381AB Sample numbers) 4107522 <br /> Ethanol N D 50 ug/l 76 43-159 <br /> Methyl Tertiary Butyl Ether N D 0 5 ug/1 105 77-127 <br /> di-Isopropyl ether N D 0 5 ug/1 104 74-125 <br /> Ethyl t-butyl ether N D 0 5 ug/l 94 74-120 <br /> t-Amyl methyl ether N D 0 5 ug/1 94 79-113 <br /> t-Butyl alcohol N D 5 ug/l 79 53-147 <br /> Benzene N D 0 5 ug/1 107 85-117 <br /> 1,2-Dichloroethane N D 0 5 u9/1 113 77-132 <br /> Toluene N D 0 5 ug/l 98 85-115 <br /> 1,2-Dibromoethane N D 0 5 ug/1 94 81-114 <br /> Ethylbenzene N D 0 5 ug/l 103 82-119 <br /> Xylene (Total) N D 0 5 ug/l 105 84-120 <br /> 'Isatch number M032382AA Sample number(s) 4107519-4107521 <br /> Ethanol N D 50 u9/1 82 43-159 <br /> Methyl Tertiary Butyl Ether N D 0 5 ug/l 99 77-127 <br /> di-Isopropyl ether N D 0 5 u9/1 106 74-125 <br /> ' Ethyl t-butyl ether N D 0 5 ug/1 103 74-120 <br /> t-Amyl methyl ether N D 0 5 ug/1 98 79-113 <br /> t-Butyl alcohol N D 5 ug/l 71 53-147 <br /> Benzene N D 0 5 ug/l 105 85-117 <br /> 1,2-Dichloroethane N D 0 5 ug/l 94 77-132 <br /> ' Toluene N D 0 5 ug/l 99 85-115 <br /> 1,2-Dibromoethane N D 0 5 ug/l 94 81-114 <br /> Ethylbenzene N D 0 5 ug/l 99 82-119 <br /> Xylene (Total) N D 0 5 ug/l 101 84-120 <br /> Sample Matrix Quality Control <br /> Ms MSD MS/MSD RPD BKG DUP DUP Dup <br /> RPD <br /> ' Analysis ame REC $RBC imits RPD AXAX cont Conc B—PD ax <br /> Batch number 03237Ao7C Sample number(s) 4107519 <br /> TPH-GRO - Waters 117 70-130 <br /> ' Batch number 032410017A Sample numbers) 4107519-4107522 <br /> Methanol (by Direct Injection) 96 96 78-116 0 20 <br /> Batch number N032381AB Sample number(s) 4107522 <br /> Ethanol 93 92 34-163 1 30 <br /> Methyl Tertiary Butyl Ether 106 101 69-134 2 30 <br /> ' di-Isopropyl ether 104 110 75-130 6 30 <br /> Ethyl t-butyl ether 96 100 73-123 4 30 <br /> *-Outside of specification <br /> ' (1) The result for one or both determinations was less than five times the LOQ <br /> �) The background result was more than four times the spike added <br />