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110 2nd Arcnuc South,#D7,Pncheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Pax 925 798 1672 <br /> Website www rmcairipbefl coin E natl ntanr(>x t.ampbell ccm <br /> QC 5UMMARY REPORT FOR SW8260B <br /> W O Sample Matrix Water QC Matrix Water WorkOrder 0509601 <br /> EPA Method SW0260B Extraction SW5030B BatchlD 18245 Spiked Sample ID 0509801-0038 <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Ng/L pg/L % Rea %Rae % RPD % Rea % Rea %RPD MS/MSD I LCS I LCSD <br /> Methyl-1-butyl ether(MTBE) ND 10 113 106 695 107 114 647 70- 130 70-130 <br /> %SSI 104 10 105 102 340 106 105 0 710 70-130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> BATCH 18245 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0509601-0013 9127/05 9 57 AM 9/29105 9129105 5 23 AM 0509601-10213 9/27105 10 27 AM 9/29/05 9129/05 6 05 AM <br /> 0509601-00313 9127/05 11 39 AM 9/29105 9/29/05 6 48 AM 0509601-004B 9/27105 10 59 AM 9129105 9129/05 7 31 AM <br /> 0509601-005B 9/27105 12 11 PM 9129105 9/29/05 8 13 AM 0509601-006B 9/27105 1 15 PM 9/29/05 9/29/05 8 56 AM <br /> 0509601-007B 9127105 8 34 AM 9/29105 9129/05 9 38 AM 0509601-008B 9127/05 9 10 AM 9/29/05 9129/05 3 47 PM <br /> F <br /> MS=Matrix Spike,MSD=Matnx Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100.(MS-Sample)I(Amount Spiked) RPD=100'(MS- MSD)I((MS+MSD)/2) <br /> MS I MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance cntena due to one or more of the following reasons a)the sample Is inhomogenous AND <br /> contains significant concentrations of analyto relative to tete amount spiked or b)the spiked sample's matrix interferes with the spike recovery <br /> NIA=not anough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration In sample exceeds spike amount far soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> 1horatory extraction solvents such as methylene chloride and acetone may occasional) appear in the method blank at low levels <br /> DHS Certification No 1644 QA/QC Officer <br />