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McCampbell Analytical, Inc. lip 2ndp venue South #I)7 Pacheco CA 94553 5560 <br /> 7cle hone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell corn E mail mam@mccampbeli com <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 07/15/04 <br /> 837 Shaw Road Date Received 07/16/04 <br /> Client Contact Tim Cuellar Date Extracttd 07/16/04 <br /> Stockton,CA 95215 <br /> Client—PO Date Analyzed 07/20/04 <br /> Lead by Graphite Furnace Atonuc Absorption* <br /> xtmrtion method E200 9 Analytical incthods E200 9 Work OiJ,r 0407214 <br /> Lab ID Client ID Matrix Extraction Lead Dl %SS <br /> 0407214-OOID Influent W TTLC ND 1 N/A <br /> t I <br /> Reporting Limit for DP=1, W TTLC 0 005 mg/L <br /> ND means not detected at or <br /> above the reporting lima S TTLC NA mg/kg <br /> 'water/product/oil/non-aqueous liquid samples and all TCLP/STLC/DiSTLC/SPLP extracts are reported in mg/L sotUsludge/solid samples In mg/kg, <br /> wipe samples inµg/wipe,filter samples inµg/filter <br /> #means surrogate recovery outside of acceptance range due to matrix interference,&means surrogate diluted out of acceptance range,ND means not <br /> detected above the reporting limit,N/A means not applicable to this sample or instrument <br /> Analytical Methods EPA 601 OC/200 7 for all elements except 200 9(water/liquid-Sb,As,Pb,Se,Tl),245 1 (Hg),7010 <br /> (sludge/soil/soltd/oillproduct/wipe/filter-As,Se,Tl),7471 B(Hg) <br /> i)liquid sample that contains greater than--1 vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,j)reporting limit raised due to insufficient sample amount,k)results are reported by dry weight,y) <br /> estimated values due to low surrogate recovery,z)reporting limit raised due to matrix interference <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />