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McCampbell Analytical, Inc. 110 2nd Avenue South #D7,Pacheco CA 94553 5560 <br /> Telephone 925-798 1620 Fax 925-798-1622 <br /> L4 <br /> Website www mccampbell cam Email roam c@mccampbell cam <br /> QC SUMMARY REPORT FOR SW8015C <br /> W O Sample Matrix Water OC Matrix Water WorkOrder 0506567 <br /> EPA Method SW8015C Extraction SW3510C BatchlD 16935 Spiked Sample ID NIA <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria <br /> pg/L pglL %Rec %Rec % RPD %Rec %Rec %RPD MS!MSD LCS 1 LCSD <br /> TPH(d) NIA 1000 NIA N/A N/A 109 110 1 09 N/A 70- 130 <br /> %SS N/A 2500 NIA N/A N/A 100 101 0 638 NIA 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> BATCH 16935 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0506567-005A 6/29/05 9 07 AM 6130/05 7/02/05 1 52 AM 0506567-006A 6/29105 9 23 AM 6130105 7!02/05 5 12 AM <br /> 0506567-007A 6129/05 9 40 AM 6130/05 7/02/05 6 18 AM 0506567-008A 6/29105 10 02 AM 6/30/05 7102/05 7 25 AM <br /> 0506567-009A 6129/05 1 12 PM 6130105 7102105 8 32 AM 0506567-OIOA 6/29/05 1 24 PM 6130/05 7102105 9 38 AM <br /> 0506567-011 a 6129105 1 39 PM 6130105 7/06105 8 18 AM 0506567-012A 6/29105 1 55 PM 6130/05 7106105 2 31 AM <br /> 0506567-013A 6/29/05 10 55 AM 6130105 7106105 12 11 AM 0506567-014A 6/29/05 11 08 AM 6/30/05 7102105 2 10 PM <br /> 0506567-015A 6/29/05 11 27 AM 6130/05 7106/05 3 41 AM 0506567-016A 6/29105 11 47 AM 6130105 7102/05 4 26 PM <br /> 0506567-017A 6129/05 9 29 AM 6130/05 7102/05 5 33 PM 0506567-018A 6/29/05 9 09 AM 6130105 7106105 4 50 AM <br /> 0506567-019A 6/29105 10 29 AM 6130105 7/02/05 6 41 PM 0506567-020A 6/29105 10 55 AM 6130105 7106/05 7 09 AM <br /> 0506567-021A 6/29105 11 26 AM 6/30105 7106/05 5 59 AM <br /> MS=Matnx Spike,MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPR=Relative Percent Deviation <br /> %Recovery=100.(MS-Sample)I(Amount Spiked) RPD=100'(MS- MSD)1((MS+MSD)12) <br /> MS 1 MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance critena due to one or more of the following reasons a)the sample is inhomogenous <br /> AND contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample s matrix interferes with the spike recovery <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for sod matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte <br /> content <br /> DHS Certification No 1644QA/QC Officer <br />