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0Ui <br /> 1102nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925 798 1620 Fax 425 795-1622 <br /> Website www mccampbell com E mail mani@rnccampbell corn <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 03/28/05 <br /> 837 Shaw Road Date Received 03/29/05 <br /> Client Contact Tim Cuellar Date Extracted 04101105-04105105 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 04/01105-04105105 <br /> Oxygenates and BTEX by GCIMS* <br /> Extraction Method SW5030B Analytical Method SW8260R Work Order 0503501 <br /> Lab ID 0503501-029B 0503501-030B 3 0503501-031B 0503501-032B <br /> Client ID MW-19B MW-20A MW-20B CSA#1 <br /> Reporting Limit for <br /> I <br /> DF=1 <br /> Matrix W W W I W <br /> DF 1 20 1 i S W <br /> Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND<10 ND ND NA 05 <br /> Benzene ND ND<10 ND ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND 200 ND ND NA 5 0 <br /> Dusopropyl ether(DIFE) ND ND<10 ND ND NA 0 5 <br /> Ethanol ND ND<1000 ND ND [NA 50 <br /> Ethylbenzene ND ND<10 ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND<10 ND ND NA 0 5 <br /> Methanol ND ND<10,000 ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND 440 1 7 ND NA 05 <br /> Toluene ND ND<10 ND ND NA 0 5 <br /> Xylenes ND ND<10 ND ND NA 05 <br /> Surrogate Recoveries{%) <br /> %SS1 117 98 101 103 <br /> %SS2 81 103 104 100 <br /> %SS3 115 f20 112 109 <br /> Comments <br /> *water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,productloillnon-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in jig/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,i)sample diluted due to high <br /> ,,game contentlmatrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting limit raised due to insufficient sample amount,n2 results are reported on a dry weight basis, see attached narrative <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br />