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r: <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> �--: MCCAUTBELL ANALYTICAL INC. Telephone;925-798-1620 Fax:925-798-1622 <br /> hLtp://www.mccampbell.co E-mail:main@mccampbell.com <br /> �= Advanced GeoEnvironmental Client Project ID:Flag City Chevron Date Sampled: 08/30/00 <br /> 4005 North Wilson Way Date Received: 08/31/00 <br /> f <br /> Stockton,CA 95205 Client Contact:Tim Cuellar Date Extracted: 09101-09106/00 <br /> Client P.O: Date Analyzed: 09101-09706100 <br /> . 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 46435 46436 46437E6438 <br /> MWl/08-30- MW2/08-30- MW4/08-30- 0- Reporting Limit <br /> Client ID 00 00 00rMatrix W W W 5 W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND<100 ND ND ND 5.0 1.0 <br /> r' Ethyl tert-Butyl Ether(ETBE) ND<100 ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) 3500 ND 1.7 ND 5.0 1.0 <br /> j tert-Amyl Methyl Ether(TAME) ND<100 ND ND ND 5.0 1.0 <br /> > tert-Butanol ND<500 ND ND ND 25 5.0 <br /> Methanol ND<20'000 ND ND ND 1000 200 <br /> F i <br /> Ethanol ND<5000 ND ND ND 250 50 <br /> r <br /> Surrogate Recoveries(%) <br /> i <br /> Dibromofluoromethane 94 93 91 92 <br /> i - Comments: <br /> i <br /> water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> r (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> 7 <br /> F <br /> 4 <br /> t^ <br /> k DHS Certification No. 1644 /Edward Hamilton,Lab Director <br /> r <br />