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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> r—. McCANDBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> h ://www.mccam bell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Flag City Chevron Date Sampled: 08/30/00 <br /> 4005 North Wilson Way Date Received: 08/31/00 <br /> Stockton,CA 95205 Client Contact:Tim Cuellar Date Extracted: 09/01-09/06/00 <br /> j Client P.O: Date Analyzed: 09/01-09/06/00 <br /> 1 <br /> EPA method 8260 modified 7 Oxygenated Volatile Organics By GC/MS <br /> Lab 1D 46447 ;30-00 <br /> 448 46449 <br /> MW9C/08-30- M0D/08- MW10E/08- Reporting Limit <br /> Client ID 00 30-00 <br /> Matrix W W W S W <br /> i# <br /> Compound Concentration* ug/kg ug/L <br /> { Di-isopropyl Ether(DIPE) ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND 5.0 1.0 <br /> " Meth 1-tert Butyl Ether(MTBE) <br /> ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND 25 5.0 <br /> Methanol ND ND ND1000 200 <br /> Ethanol ND 120 ND 250 50 <br /> G <br /> F+ Surrogate Recoveries(%) <br /> Dibromofluoromethane 9'7 9$ gg � <br /> F <br /> Comments: <br /> f <br /> F <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;6)sample diluted due to <br /> high organic content <br /> �k <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />