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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> —` McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> http://www.mccWTbell.com E-mail:main@mccampbell.com <br /> P ` <br /> Advanced GeoEnvironmental Client Project ID:Flag City Date Sampled. 08/29/00 <br /> r 4005 North Wilson Way Date Received: 08/30/00 <br /> Stockton,CA 95205 Client Contact: Tim Cuallar Date Extracted: 08/31-09106/00 <br /> Client P,O: Date Analyzed: 08/31-09/06/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 46253 46254 46255 46256 <br /> 4 MW-13A/08- MW-13B/08- MW-13C/08- MW-13D/09- Reporting Limit <br /> Client ID 29-00 29-00 29-00 29-00 <br /> rw <br /> Matrix W W W W S w <br /> r Compound Concentration* ug/kg ug/L <br /> F Di-isopropyl Ether(D1PE) ND<2.5 ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND<2.5 ND ND ND 5.0 1.0 I <br /> 't Methl-tert Butyl Ether <br /> y ty (MTBE) 77 ND ND ND 5.0 1.4 <br /> tert-Amyl Methyl Ether(TAME) ND<2.5 ND ND ND 5.0 1.0 <br /> tert-Butanol ND<13 ND ND 53 25 5.0 <br /> �. Methanol ND<500 ND ND ND 1000 200 <br /> Ethanol 9100 99 ND ND 250 50 <br /> Surrogate Recoveries <br /> I <br /> Dibromofluoromethane 96 93 90 88 <br /> t i <br /> Comments: I� <br /> I <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> [ ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis ` <br /> P (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> 4 <br /> high organic content <br /> F 4 <br /> DHS Certification No. 1644 /� Edward Hamilton,Lab Director <br />