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Inc. 102nd Avenue South 4D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical, nc. Telephone 925-798 1620 Fax 925 798-1622 <br /> -_ - -- - - - - -- -_ - - - Website www mccampbell corn-E-mail main@mccampbell com _ <br /> Advanced GeoEnvironmental,Inc Client Protect ID Flag City Chevron Date Sampled 01120104-01122104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/24/04-01128/04 <br /> Se"d-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method. SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-014A <br /> ` Client ID P40A-15' - - - <br /> Matrix Soil <br /> Compound Concentration* DF Unit Compound Concentration * DF Ia <br /> Acenaphthene ND 10 1 033 1 Acenaphthylene ND l 0 033 <br /> Acetochlor ND 10 033 Anthracene ND 1 0 033 <br /> Benztdme ND 10 1 6 Benzoic Acid ND to 16 <br /> Benzo(a)anthracene ND 10 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 10 033 Benzo(g,hj)perylene ND 1 0 033 <br /> Benzo opyrene ND 10 033 Benzyl Alcohol ND 10 066 <br /> Bis(2-chloroethox Methane ND 1 0 033 Bis(2-chloroeth k)Ether ND 1 0 033 <br /> Bis 2-chloroisopropyl Ether ND 10 033 Bis 2-eth Ihexyi)Adipate ND 10 033 <br /> Bis 2-ethylhexyl Phthalate ND 1 0 033 4-Bromo hen I Phenyl Ether ND 10 033 <br /> Bu /ben I Phthalate ND 1 0 033 4-ChloroantEme ND 1 0 066 <br /> Nttrobenzene ND 10 16 4-Chloro-3-meth 1phenoi ND 1 0 033 <br /> 2-Chlorona hthalene ND to 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chloro hen 1 Phen i Ether ND 10 033 Ch Bene ND 1 0 033 <br /> Dibenzo a,h anthracene ND 10 033 Dibenzofutan ND 10 033 <br /> Di-n-but 1 Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 10 033 1,4-Dichlorobenzene ND to 033 <br /> • 3 3-Dichlorobenzidme ND 10 066 2 4-Dichloro henol ND 10 033 <br /> Diethyl Phthalate ND 1 0 033 2,4-Dimethylphenol ND 10 033 <br /> Dimeth 1 Phthalate ND 10 033 4,6-Dinitro-2-meth 1 henol ND 10 16 <br /> 2,4-Dinitro henol ND 1 0 1 6 2,4-Dinitrotoluene ND l 0 033 <br /> 2,6-Dimtrotoluene ND 1 0 033 Di-n-oct 1 Phthalate ND 1 0 033 <br /> 1,2-Dt hen lh drazine ND 10 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 10 0 33 1-lexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadicne ND 1 0 033 Hexachloroc clo entadiene ND 1 0 1 6 <br /> Hexachloroethane ND 1 0 0 33 Indeno(1,2,3-cd)pyrene ND 1 0 033 -- <br /> Isophorone ND 10 033 2-Meth lna hthalene ND l 0 0 33 <br /> 2-Methyl henoi(o-Cresol ND 10 033 3 Wor 4-Meth I henol m, -Cresol) ND 1 0 033 <br /> Naphthalene ND 10 033 2-Nitroanilme ND 10 1 6 <br /> 3-Nitroaniline ND 10 16 4-Nitroanilme ND 10 16 <br /> 2-Nitrophenol ND 10 1 6 4-Nitrohent ND 10 033 <br /> N-Nitrosodt hen lamme ND 10 033 N-Nitrosodi-n-propyiamine ND 10 033 <br /> Pentachlorophenol ND to 1 6 Phenanthrene ND 10 033 <br /> Phenol ND 10 033 Pyrene ND 1 0 033 <br /> 1,2,4-Tnchlorobenzene ND 10 0 33 2,4 5-Trichlorophenol ND 1 0 033 <br /> 2 4 6-Tnchloro henol ND 1 0 033 <br /> Surrogate Recoveries(%) <br /> %SSI 106 %SS2 108 <br /> %SS3 899 %SS4 93 0 <br /> SS5 928 %SS6 979 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in gg/L,soillsludgelsohd samples in mg/kg,wipe samples inµg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matnx interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> coneentratlon but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />