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110 2nd Avenue South,ND7,Pacheco CA 94553-5560 <br /> McCain bell Anal tical Inc. Telephone 925-798-1620 Fax 925 798 1622 <br /> -� n1�24 -_— — —� --- - ---— -- ——Website www mecampbell com E mail mamQmecampbell com ---- <br /> Advanced <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01120/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/24104-01/28/04 <br /> Serpi-Volatile Organics by GC/MS(Baste Target List)* <br /> Extraction Method SW35W Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-022A <br /> Client ID P42-25' <br /> Matrix Soil <br /> ig <br /> Compound Concentration* DF LO„n,'i' Compound Concentration* DF eLMM <br /> a <br /> Acenaphthene ND 1 0 033 Acenaphthylene ND 1 0 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 16 Benzoic Acid ND l 0 16 <br /> Benzo(a)anthracene ND 10 033 Benzo b fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 .033 l3enzo(g,h,i)pCiylenc ND 10 033 <br /> Benzo a ene ND 1 0 033 Benzyl Alcohol ND 1 0 066 <br /> Bis(2-chloroethox Methane ND l 0 033 Bis(2-chloroeth 1)Ether ND 1 0 033 <br /> Bis 2-chloroiso ro l Ether ND 10 033 Bis 2-eth lhexylj Adi ate ND 1 0 033 <br /> Bis(2-eth [hex 1 Phthalate ND 1 0 033 4-Bromo hen I Phenyl Ether ND 1 0 033 <br /> Butylbenzyl Phthalate ND 1 0 033 4-Chloroaniline ND l 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-meth l henol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chloro hen l Phenyl Ether ND 1 0 0 33 Ch Bene ND 1 0 033 <br /> Dibenzo(a,h)anthracene ND 10 033 Dibenzolluran ND 1 0 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 0 33 <br /> 0 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 033 <br /> 3,3-Dichlorobenzidine ND 1 0 066 2,4-Dichloro hent ND 1 0 033 <br /> Dieth t Phthalate ND 1 0 033 2,4-Dlmeth l henol ND 1 0 033 <br /> Dimethyl Phthalate ND 10 033 4,6-Dmitro-2-meth l henol ND 1 0 l 6 <br /> 2,4-Dinitrohenol ND l 0 16 2,4-Dmitrotoluene ND 1 0 rO 33 <br /> 2,6-Dinarotoluene ND 1 0 033 Di-n-octyl Phthalate ND 1 0 033 <br /> 1,2-Di henylh drazine ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 HexachlorocycloLmritathene ND 1 0 1 6 <br /> Hexachloroethane ND l 0 033 Indeno 1,2,3-cd e ND 1 0 033 <br /> Iso horone ND 1 0 033 2-Meth Ina hthalene ND 10 033 <br /> 2-Meth 1 henol(o-Cresol) ND 10 0 33 3&/or 4-Meth Iphenal (m,—Cresol) ND 1 0 033 <br /> Naphthalene ND 10 033 2-Nitroanilme ND 1 0 16 <br /> 3-Nitroaniline ND 10 16 4-Nttroanilme ND 10 16 <br /> 2-Nitrophenol ND 10 16 4-Nitro henol ND 1 0 033 <br /> N-Nrtrosodi hen lamme ND 10 033 N-Nttrosodi-n-propylamme ND 10 033 <br /> Pentachlorophenol ND 1 0 16 Phenanthrene ND 1 0 033 <br /> Phenol ND 1 0 033 Pyrene ND 1 0 033 <br /> 1,2,4-Trich[orobenzen ND 10 033 2,4,5-Tnehloro henol ND 1 0 033 <br /> 2 4 6-Trichloro henol ND 1 0 F 033 <br /> Surrogate Recoveries(%) <br /> %SSI 937 %SS2 868 <br /> %SS3 852 %SS4 828 <br /> %SS5 869 %SS6 874 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in gglL,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,product/od/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matnx interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />