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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell com E-mail mamQa mccampbell com <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 06/15/04 <br /> 837 Shaw Road Date Received 06/16/04 <br /> Client Contact Tim Cuellar Date Extracted 06/16/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 06/16/04 <br /> Lead by Graphite Furnace Atomic Absorption* <br /> Extraction method F200 9 Analytical methods E200 9 Work Order 0406263 <br /> Lab ID Client I_D Matrix Extraction Lead DF %SS <br /> 0406263-OIOD Influent W TTLC ND I N/A <br /> 0406263-011D Effluent W TTLC ND I NIA <br /> i <br /> Reporting Limit for DF=l, W TTLC 0 005 ing/L <br /> ND means not detected at or <br /> above the reporting limit S TT'LC NA mg/kg <br /> *water/product/oillnon-aqueous liquid samples and all TCL?!STLC/DISTLC/SPLP extracts are reported in mg/L,soil/sludge/solid samples in mglkg, <br /> wipe samples in pg/wipe,filter samples in pg/filter <br /> #means surrogate recovery outside of acceptance range due to matrix interference,&means surrogate diluted out of acceptance range,ND means not <br /> detected above the reporting limit,N/A means not applicable to this sample or instrument <br /> Analytical Methods EPA 601OC/200 7 for all elements except 200 9(water/liquid-Sb,As,Pb,Se,TI),245 1 (Hg),7010 <br /> (Sludge/so4/sohd/oillproduct/wipe/filter-As,Se TI),7471B(Hg) <br /> i)liquid sample that contains greater than—1 vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,j)reporting limit raised due to insufficient sample amount,k)results are reported by dry weight,y) <br /> estimated values due to low surrogate recovery,z)reporting limit raised due to matrix interference <br /> • <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br /> w <br />