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NE1.,AP Certification 01103CA FLAP Certification 1664 Caltest ' ENVIRONMENTAL ANAL'Y'SES LAB ORDER No C120219 ORGANIC ANALYTICAL RESULTS Page 6 of 7 ANALYTE RESULT R L MDL UNITS D F ANALYZED QC BATCH NOTES LAB NUMBER C120219 1 (continued) SAMPLE ID FLAG CITY CHEV EFF SAMPLED 05 DEC 02 14 3B METHOD EPA 625 SEMIVOLATILE ORGANIC COMPOUNDS 1 12 17 02 S020107BNA (continued) Nitrobenzene NO 1 0 7 ug/L N-Nitrosodimethylamine NO 5 0 6 ug/L N-Nitrosodiphenylamine ND 1 0 7 ug/L N-Nitrosodi-n-propylamine NO 5 0 8 ug/L 4-Chloro-3-methylphenol NO 1 0 5 ug/L 2-Chlorophenol NO 2 0 6 ug/L 2 4-Dichlorophenol NO 1 0 7 ug/L 2 4-Dimethylphenol ND 2 0 9 ug/L 2 4-Dim trophenol NO 5 0 6 ug/L 2-Methyl-4 6-dinitrophenol NO 5 0 9 ug/L 2-Nitrophenol NO 5 0 7 ug/L 4-Nitrophenol NO 5 0 6 ug/L. ntachlorophenol ND 5 1 ug/L enol NO 1 0 4 ug/L 2 4 6-Trichlorophenol NO 5 0 6 ug/L Surrogate Nitrobenzene-d5 63 % Surrogate 2-Fluorobiphenyl 61 % Surrogate Terphenyl-d14 86 % Surrogate 2-Fluorophenol 49 % Surrogate Phenol-d6 34 % Surrogate 2 4 6-Tribromophenol 83 % LAB NUMBER 0120219-1 (continued) SAMPLE ID FLAG CITY CHEV EFF SAMPLED 05 DEC 02 14 38 METHOD EPA 624 VOLATILE ORGANIC COMPOUNDS 1 12 14 02 V020139MSB 1 2 3 Acrolein NO 5 1 ug/L Acrylonitrile NO 2 1 ug/L Benzene NO 0 5 0 3 ug/L Bromodichloromethane NO 0 5 0 2 ug/L Bromoform ND 0 5 0 2 ug/L Bromomethane (Methyl Bromide) ND 0 5 0 42 ug/L Carbon Tetrachloride NO 0 5 0 42 ug/L 1) Sample Preparation on 12-13-02 using EPA 624 2) 'RL' (Reporting Limit) represents the lowest calibration standard in methods that require multipoint calibrations RL is equivalent to the ML (Minimum Level) in the State Implementation Plan (SIP) of the California Toxics Rule (CTR) Analytes reported as ND' were not detected at or above the listed Method Detection Limits (MDL) 1885 North Kelly Road • Napa, California 94558 (707)258-4000 • Fax (707)226-1001 • e-mail caltest@caltestlab corn otr