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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br />' McCatnpbell Analytical Inc Telephone 925-798-1620 Fax 925-79&1622 <br /> 7httP//wwwmccampbellconi E-mail mam(rdmceainpbell corn <br /> C SUMMARY REPORT <br /> Q FOR SW8260B <br /> Matrix W WorkOrder 0303448 <br /> EPA Method SW8260B Extraction SW5030B BatchlD 6312 Spiked Sample ID NIA <br /> Compound Sample Spiked MS* MSD" MS-MSD* LCS LCSD LCS-LCSD Acceptance Catena(%) <br /> jrg/L Ng/L %Rec %Rec %RPD %Rec %Rec %RPD Low J High <br /> Dnsopnopylether(DIPE) N/A 10 N/A N/A N/A 120 119 121 70 130 <br />' Ethyl tert-butyl ether(FTSE) NIA 10 N/A N/A N/A 103 102 5 53 70 130 <br /> Methyl-t-butyl ether(MTBE) N/A 10 N/A N/A N/A 111 Ill 1 60 70 130 <br /> tert-Amyl methyl ether(TAME) N/A 10 N/A N/A N/A 975 976 389 70 m 1301 <br /> Methanol N/A 2500 N/A N/AqN/A99 <br /> 09 117 229 70 130 <br />' Ethanol NIA SOD NIA N/A14 111 0 467 70 130 <br /> 1,2-Dibromoethane(EDB) N/A t0 N/A N/A 3 100 257 70 130 <br /> 1,2-Dtchloroethane(1,2-DCA) N/A 10 N/A NIA N/A 110 109 632 70 130 <br /> %SS NIA 100 NIA N/A NIA 103 102 219 7O 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> I <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent <br /> Deviation <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for sod matnx or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or <br /> Ianalyte content. <br /> %Recovery=100"(MS-Sample)I(Amount Spiked),RPD=100`(MS—MSD)/(MS+MSD)12 <br /> "MS and/or MSD spike recoveries may not be near 100%or the RPDs near 0%it a)the sample is inhomogenous AND contains significant concentrations of <br /> analyte relative to the amount Spiked or b)d that specific sample matrix interferes with spike recovery <br />