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110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCalnpbell Analytical Inc Telephone 925-798 1620 Fax 925-798-1622 <br /> - — T ht /lwww nrcampbell cam F-mail main ca bell com <br /> Advanced GeoEnvlronmental, Inc Client Project ID Flag City Chevron Date Sampled 12/05/02 <br />' 837 Shaw Road Date Received 12/06/02 <br /> Client Contact Tun Cuellar Date Extracted 12/11/02-12/12/02 <br /> Stockton,CA 95215 <br />' Client P O Date Analyzed 12/11/02-I2/12/02 - <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> ExtracuonMethod SW50308 Analytical Method SW82604 Work Order 0212097 <br />' Lab 1D 0212097-013C 0212097-014C 0212097-015C <br /> Client 1D MW10c MW10d MW10e Reporting Limit for <br />' Matrix W W W DF-1 <br /> i <br /> Compound Concentration ug/kg µg/L <br />' Dusopropyl ether(DIPE) ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) ND ND ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND NA 50 <br /> Methanol ND ND ND NA 500 <br /> Ethanol ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 114 115 114 <br /> Comments <br /> I *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soiUsludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hanulton, Lab Director <br />