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NELAP Certification 01103CA ELAP Certification 1664 <br /> Caltest <br /> ANA 1.111 CAL L%Ro RATO R) <br /> ENviR0NMENTAL ANALYSES <br /> LAB ORDER No f C090171 <br /> ORGANIC ANALYTICAL RESULTS Page 3 of 7 <br /> ANALYTE RESULT R L MDL UNITS D F ANALYZED QC BATCH NOTES <br /> LAB NUMBER C090171 1 <br /> SAMPLE ID EFFLUENT FLAG CITY CHEVRON <br /> SAMPLED 05 SEP 02 13 10 <br /> METHOD EPA 608 <br /> CHLORINATED PESTICIDES & PCBS 1 09 17 02 T0202590CP 1 2 3 4 <br /> Aldrin NO 0 005 0 003 ug/L <br /> alpha-BHC ND 0 01 0 003 ug/L <br /> r beta-BHC ND 0 005 0 004 ug/L <br /> -- gamma-BHC (Lindane) ND 0 01 0 003 ug/L <br /> delta-BHC ND 0 005 0 002 ug/L <br /> Chlordane NO 0 02 0 005 ug/L <br /> p p -DDD NO 0 01 0 002 ug/L <br /> —p p -DDL NO 0 01 0 002 ug/L <br /> _p p'-DDT ND 0 01 0 003 ug/L <br /> — Dieldrin ND 0 01 0 002 ug/L <br /> ­z Endosulfan I ND 0 01 0 002 ug/L <br /> Endosulfan II ND 0 01 0 002 ug/L <br /> Endosulfan Sulfate ND 0 01 0 002 ug/L <br /> drin ND 0 01 0 002 ug/L <br /> drin Aldehyde NO 0 01 0 002 ug/L <br /> Endrin Ketone NO 0 01 0 002 ug/L <br /> Heptachlor ND 0 01 0 003 ug/L <br /> -� Heptachlor Epoxide ND 0 01 0 003 ug/L <br /> t Methoxychlor NO 0 01 0 003 ug/L <br /> Toxaphene ND 0 5 0 4 ug/L <br /> t' PCB 1016 NO 0 1 0 05 ug/L <br /> PCB 1221 ND 0 1 0 03 ug/L <br /> PCB 1232 ND 0 1 0 04 ug/L <br /> PCB 1242 ND 0 1 0 05 ug/L <br /> PCB 1248 NO 0 1 0 05 ug/L <br /> PCB 1254 ND 0 1 0 07 ug/L <br /> PCB 1260 ND 0 1 0 05 ug/L <br /> Surrogate TCMX 67 % <br /> Surrogate Decachlorobiphenyl 89 % <br /> LAB NUMBER C090171 1 (continued) <br /> SAMPLE ID EFFLUENT FLAG CITY CHEVRON <br /> SAMPLED 05 SEP 02 13 10 <br /> METHOD EPA 507 <br /> EPA 507 ORG NIT/ORG PHOS PEST 1 09 24 02 T020264OPP 3 5 <br /> Atrazine NO 0 1 0 06 ug/L <br /> 1) Sample Preparation on 09-10-02 using EPA 608 <br /> 16RL' (Reporting Limit) represents the lowest calibration standard in methods that require multipoint calibrations RL is <br /> equivalent to the ML (Minimum Level) in the State Implementation Plan (SIP) of the California Toxics Rule (CTR) <br /> 3) Analytes reported as 'ND were not detected at or above the listed Method Detection Limits (MDL) <br /> 4) This sample was analyzed following Florisil column cleanup (EPA Method 36208) <br /> 5) Sample Preparation on 09-13-02 using EPA 507 <br /> 1885 North Kelly Road • Napa, California 94558 v� <br /> (707)258-4000 • Fax (707)226-1001 • e-mail caltest@caltestlab com <br />