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NELAP Certification 01103CA ELAP Certification 1664 <br /> Caltest ; <br /> ENVIRONMENTAL ANALYSES <br /> LAB ORDER No C09G171 <br /> ORGANIC ANALYTICAL RESULTS Page 6 of 7 <br /> ANALYTE RESULT R L MDL UNITS D F ANALYZED QC BATCH NOTES <br /> LAB NUMBER C090171-1 (continued) <br /> SAMPLE ID EFFLUENT FLAG CITY CHEVRON <br /> SAMPLED 05 SEP 02 13 10 <br /> METHOD EPA 625 <br /> SEMIVOLATILE ORGANIC COMPOUNDS 1 09 17 02 S020072BNA <br /> (continued) <br /> Nitrobenzene ND 1 0 7 ug/L <br /> N-Nitrosodimethylamine NO 5 0 6 ug/L <br /> -� N-Nitrosodiphenylamine NO 1 0 7 ug/L <br /> T N-Nitrosodi-n-propylamine ND 5 0 B ug/L <br /> -cv- 4-Chloro-3-methylphenol NO 1 0 5 ug/L <br /> �-- 2-Chlorophenol NO 2 0 6 ug/L <br /> --2 4-Dichlorophenol NO 1 0 7 ug/L <br /> 2 4-Dimethylphenol NO 2 0 9 ug/L <br /> 2 4-Dim trophenol NO 5 0 6 ug/L <br /> —-2-Methyl-4 6-dinitrophenol ND 5 0 9 ug/L <br /> 2-Nitrophenol ND 5 0 7 ug/L <br /> --4-Nitrophenol ND 5 0 6 ug/L <br /> 0ntachlorophenol NO 5 1 ug/L <br /> enol ND 1 0 4 ug/L <br /> 2 4 6-Trichlorophenol NO 5 0 6 ug/L <br /> Surrogate Nitrobenzene-6 49 % <br /> Surrogate 2-Fluorobiphenyl 42 % <br /> Surrogate Terphenyl-d14 114 % <br /> Surrogate 2-Fluorophenol 34 % <br /> Surrogate Phenol-d6 25 % <br /> Surrogate 2 4 6-Tribromophenol 67 % <br /> LAB NUMBER C090171 1 (continued) <br /> SAMPLE ID EFFLUENT FLAG CITY CHEVRON <br /> SAMPLED 05 SEP 02 13 10 <br /> METHOD EPA 624 <br /> VOLATILE ORGANIC COMPOUNDS 1 09 18 02 V020114MSA 1 2 3 <br /> Acrolein NO 5 1 ug/L <br /> Acrylom trite ND 2 1 ug/L <br /> Benzene ND 0 5 0 3 ug/L <br /> Bromodichloromethane ND 0 5 0 2 ug/L <br /> Bromoform NO 0 5 0 2 ug/L <br /> Bromomethane (Methyl Bromide) ND 0 5 0 42 ug/L <br /> r Carbon Tetrachloride NO 0 5 0 42 ug/L <br /> 1) Sample Preparation on 09-17-02 using EPA 624 <br /> 2) 'RL (Reporting Limit) represents the lowest calibration standard in methods that require multipoint calibrations RL is <br /> iequivalent to the ML (Minimum Level) in the State Implementation Plan (SIP) of the California Toxics Rule (CTR) <br /> Analytes reported as NO were not detected at or above the listed Method Detection Limits (MDL) <br /> 1885 North Kelly Road • Napa, California 94558 401 <br /> (707)258-4000 • Fax (707)226-1001 • e-mail caltest@caltestlab com Imd0 <br />