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NELAP Certification 01103CA ELAP Certification 1664 <br /> Caltest <br /> ANAL111CAL LABORATORY <br /> . ENVIRONMENTAL ANALYSES <br /> LAB ORDER No C090171 <br /> LABORATORY CONTROL SAMPLE ANALYTICAL RESULTS Page 10 of 16 <br /> SPIKE SPIKE\DUP SPK\DUP ACCEPTANCE REL% <br /> ANALYTE AMOUNT RESULT %REC %REQ \RPD DIFF ANALYZED NOTES <br /> QC BATCH S020072BNA <br /> SEMIVOLATILE ORGANIC COMPOUNDS 09 16 02 <br /> 2 4-Dinitrotoluene 50 0 40 8\ 82\ 30-130\ <br /> N-Nitrosodi-n-propylamine 50 0 32 9\ 66\ 30-130\ <br /> 4-Chloro-3-methylphenol 100 60 4\ 60\ 10-130\ <br /> 2-Chlorophenol 100 50 3\ 50\ 28-1171 <br /> 4-N7trophenol 100 42 4\ 42\ 20-120\ <br /> Pentachlorophenol 100 94 8\ 95\ 20-140\ <br /> Phenol 1.00 26 7\ 27\ 20-120\ <br /> Surrogate Nitrobenzene-d5 50 0 29 0\ 58\ 20-120\ <br /> Surrogate 2-Fluorobiphenyl 50 0 24 1\ 48\ 10-1201 <br /> Surrogate Terphenyl-d14 50 0 49 5\ 99\ 30-130\ <br /> Surrogate 2-Fluorophenol 100 41 0\ 41\ 20-120\ <br /> Surrogate Phenol-d6 100 30 5\ 30\ 10-120\ <br /> Surrogate 2 4 6-Tribromophenol 100 88 8\ 89\ 30-140\ <br /> QC BATCH T020255OPP <br /> OGANOPHOSPHOROUS PESTICIDES 09 22 02 <br /> Diazinon 3 00 2 31\ 77\ 40-140\ <br /> Disulfoton (D,-Syston) 3 00 2 30\ 77\ 30-1301 <br /> Parathion methyl 3 00 2 71\ 90\ 30-130\ <br /> Surrogate-Tributylphosphate 5 00 3 59\ 72\ 20-120\ <br /> Surrogate-Triphenylphosphate 5 00 4 431 89\ 45-138\ <br /> QC BATCH T0202590CP <br /> CHLORINATED PESTICIDES & PCBS 09 16 02 1 <br /> Aldrin 0 200 0 0620\ 31\ 30-130\25 <br /> gamma-BHC (Lindane) 0 200 0 126\ 63\ 59-93\20 <br /> p p'-DDT 0 200 0 152\ 76\ 30-127114 <br /> Dieldrin 0 200 0 134\ 67\ 63-107117 <br /> Endrin 0 200 0 146\ 73\ 63-115\22 <br /> Heptachlor 0 200 0 08851 441 28-104\17 <br /> Surrogate TCMX 0 200 0 0735\ 37\ 14-78\ <br /> Surrogate Decachlorobiphenyl 0 200 0 107\ 54\ 38-115\ <br /> 1) This sample was analyzed following Florisil column cleanup (EPA Method 3620B) <br /> 1885 North Kelly Road - Napa, California 94558 416 <br /> (707)258-4000 - Fax (707)226-1001 - e-mail caltest@caltestlab corn gra <br /> i <br />