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110 2nd Avenue South !#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> littp I/www mccampbell com E-marl mmn@mecampWll com <br /> Advanced GeoEnvtronmental,Inc Client Project M Flag City Chevron Date Sampled 06/17/02 <br /> 837 Shaw Road Date Received 06/18/02 <br /> Client Contact Tam Cuellar Date Extracted 06/21/02 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 06/21/02 <br /> Semi-Volatile Organics by GC/MS* <br /> Extraction Method_ SW3510C Analytical Method SW8270D Work Order 0206276 <br /> Lab ID 0206276-001A <br /> Client 1D Ef)fluent - <br /> Matnx Water <br /> CompoundConct <br /> Concentration* DF I 1`rui s Compound I Cancentratton * DF Limit <br /> FBis <br /> idme ND 1 0 5 Bis(2-chloroetboxy)Methane ND 1 0 5 <br /> 2-chlorcethyl)Ether ND 1 0 1 i Bls(2-chloroisopropyl)Ether I ND 1 0 10 <br /> 2-ethylhexyl)Phthalate ND 1 0 5 4-Bromophenyl Phenyl Ether ! ND 1 0 10 <br /> Butylbenzyl Phthalate ND 1 0 10 4-Chloro-3-methyiphenol ND 1 0 f 5 <br /> 2-Chloronaphtbalene ND 10 10 2-Chlorophcnol ND 1 0 2 <br /> 4-Chlorophenyl Phenyl Ether ND 10 5 Di-n-butyl Phthalate ND 1 0 10 <br /> 3 3-Dichlorobenzidine I ND 1 0 5 2,4-Dichlorophenol I ND 1 0 I 1 <br /> Diethyl Phthalate ND 1 0 2 2,4-Dimethylphenol ND 1 0 2 <br /> Dimethyl Phthalate 3 ND 10 24,6-Duutro-2-methyiphcnol ND 1 0 10 <br /> 2,4-Dinitrophenol ND 10 5 2,4-Dimtrotoluene i ND 10 5 <br /> 2 6-Dinitrotoluene ND 10 5 Di-n-octyl Phthalate ND 10 10 <br /> 1,2-Diphenylhydrazine ND 10 1 Hexachlorocyelopentadiene ND 10 5 <br /> Isophorone ND 1 0 1 2 Nitrophenoi ND 1 0 10 <br /> 4-Nitrophenol ND 1 0 10 € Nitrobenzene ND 1 0 10 <br /> N-Nitrosodiphenylamine ' ND 1 0 i 1 i N-NltrosodimethyIaimne ND 1 0 5 <br /> N-Nitrosodi-n-propylamine I ND 10 5 ! Pentachlorophenol ND 1 0 1 <br /> Phenol j ND 10 1 j 2,4,6-Trichlorophenol ND 1 0 10 <br /> Surrogate Recoveries C/„) <br /> %SSi81 5 %SS2 33 6 <br /> %SS3 120 � %SS4 � 951 <br /> %SS5 118 %SS6 311 <br /> Comments <br /> '”water and vapor samples and all TCL.P&SPLP extracts are reported in ug/L soil and sludge samples in mg/kg, wipe samples in ug/wipe,oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> Organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />